C₃₄H₂₀Cl₂O₄

Base Information

• Chemical Name: C₃₄H₂₀Cl₂O₄
• CAS No.: 1629168-28-0
• Molecular Formula: C₃₄H₂₀Cl₂O₄
• Molecular Weight: 563.436
• Mol file: 1629168-28-0.mol

Synonyms:

Chemical Property of C₃₄H₂₀Cl₂O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₄H₂₀Cl₂O₄

There total 1 articles about C₃₄H₂₀Cl₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

2-chloro-4-fluorobenzaldehyde (84194-36-5) + (R)-1,1'-Bi-2-naphthol (18531-94-7) → C34H20Cl2O4 (1616959-96-6,1629168-28-0)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 15h;

DOI:10.1039/c4cc02710h

Reference yield: 77.8%

C34H20Cl2O4 (1616959-96-6,1629168-28-0) + benzil (134-81-6) → C62H40Cl2N4O2 (1629163-90-1,1629168-26-8)

Guidance literature:

With ammonium acetate; In dichloromethane; at 110 ℃; for 48h; Sealed tube;

DOI:10.1039/c4cc02710h

Reference yield:

C34H20Cl2O4 (1616959-96-6,1629168-28-0) → C62H38Cl2N4O2 (1616959-92-2,1620556-00-4,1629168-29-1)

Guidance literature:

Multi-step reaction with 2 steps

1: ammonium acetate / dichloromethane / 48 h / 110 °C / Sealed tube

2: potassium hexacyanoferrate(III); potassium hydroxide / benzene; water / 3 h / 20 °C / Inert atmosphere; Darkness

With ammonium acetate; potassium hydroxide; potassium hexacyanoferrate(III); In dichloromethane; water; benzene;

DOI:10.1039/c4cc02710h

upstream raw materials:

2-chloro-4-fluorobenzaldehyde

(R)-1,1'-Bi-2-naphthol

Downstream raw materials:

C₆₂H₄₀Cl₂N₄O₂

C₆₂H₃₈Cl₂N₄O₂