[(C₅H₅)Ti(2,6-dimethylphenyl isocyanide)4I]

Base Information

Chemical Name:[(C₅H₅)Ti(2,6-dimethylphenyl isocyanide)4I]
CAS No.:1029982-61-3
Molecular Formula:C₄₁H₄₁IN₄Ti
Molecular Weight:764.588
Hs Code.:

[(C<sub>5</sub>H<sub>5</sub>)Ti(2,6-dimethylphenyl isocyanide)4I]

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Chemical Property of [(C₅H₅)Ti(2,6-dimethylphenyl isocyanide)4I]

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Technology Process of [(C₅H₅)Ti(2,6-dimethylphenyl isocyanide)4I]

There total 1 articles about [(C₅H₅)Ti(2,6-dimethylphenyl isocyanide)4I] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 100763-16-4
[(C₂H₅)4N]⁽¹⁺⁾*[(C₅H₅)Ti(CO)4]^(1-)=[(C₂H₅)4N][(C₅H₅)Ti(CO)4]

: 119072-54-7,2769-71-3
2,6-dimethylphenyl isonitrile

: 7553-56-2,12190-71-5,8031-47-8
iodine

: 1029982-61-3
[(C₅H₅)Ti(2,6-dimethylphenyl isocyanide)4I]

Guidance literature:: In toluene; byproducts: CO; vac. line; cold toluene (-78°C) was added to mixt. of Ti complex and isocyanide; soln. of I2 in toluene was added with stirring; stirred overnight while slowly warmed to room temp.; stirred for 48 h; filtered; solvent removed (vac.); sublimed (20°C, 0.1 torr); recrystd. (toluene); elem. anal.;
DOI:10.1016/j.jorganchem.2007.11.047

Reference yield:

: 1029982-61-3
[(C₅H₅)Ti(2,6-dimethylphenyl isocyanide)4I]

: 7553-56-2,12190-71-5,8031-47-8
iodine

: 1029982-63-5
[(C₅H₅)Ti(2,6-dimethylphenyl isocyanide)2I₂]

Guidance literature:: In toluene; vac. line; Ti complex was treated with I2 (0.5 equiv.) in toluene at -65°C; warmed to room temp. with stirring over 5 h; filtered; solvent removed (vac.);;
DOI:10.1016/j.jorganchem.2007.11.047