1-(Tricyclo[2.2.1.02,6]hept-1-yl)ethanone

Base Information

Chemical Name:1-(Tricyclo[2.2.1.02,6]hept-1-yl)ethanone
CAS No.:22482-71-9
Molecular Formula:C₉H₁₂O
Molecular Weight:136.194
Hs Code.:
NSC Number:139866
DSSTox Substance ID:DTXSID00300895

Synonyms:22482-71-9;1-(tricyclo[2.2.1.02,6]hept-1-yl)ethanone;NSC139866;DTXSID00300895;NSC-139866

Suppliers and Price of 1-(Tricyclo[2.2.1.02,6]hept-1-yl)ethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 1-(Tricyclo[2.2.1.02,6]hept-1-yl)ethanone

Chemical Property:

Vapor Pressure:0.202mmHg at 25°C
XLogP3:1.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:136.088815002
Heavy Atom Count:10
Complexity:207

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)C12CC3CC1C2C3

Technology Process of 1-(Tricyclo[2.2.1.02,6]hept-1-yl)ethanone

There total 4 articles about 1-(Tricyclo[2.2.1.02,6]hept-1-yl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: Toluene-4-sulfonic acid (1S,2R,4S)-1-acetyl-bicyclo[2.2.1]hept-2-yl ester

: 22482-71-9
1-Acetyl-nortricyclen

: 95800-00-3
endo-2-acetyl-exo-bicyclo<2.2.1>heptan-2-ol

: 31457-44-0
1-(norborn-2-en-1-yl)ethanone

: 1-((1S,2R,4S)-2-Hydroxy-bicyclo[2.2.1]hept-1-yl)-ethanone

Guidance literature:: With water; In 1,4-dioxane; Product distribution;
DOI:10.1002/hlca.19880710203

Reference yield:

: 279-19-6
nortricyclane

: 75-36-5
acetyl chloride

: 22482-71-9
1-Acetyl-nortricyclen

Guidance literature:: With aluminium trichloride; dichloromethane; at 95 ℃; under 14 Torr;
DOI:10.1080/08964280109595772

Reference yield:

: 16219-75-3
2-ethylidenenorbornene

: 22482-71-9
1-Acetyl-nortricyclen

Guidance literature:: Multi-step reaction with 2 steps

1: (AcO)2Hg / tetrahydrofuran; H₂O

2: Na₂Cr₂O₇, aq. H₂SO₄

With sodium dichromate; sulfuric acid; mercury(II) diacetate; In tetrahydrofuran; water;