Pb₂(N-((1-pyridin-2-yl)benzylidene)-N'-[2-(4-[2-[((1-pyridin-2-yl)benzylidene)amino]ethyl]piperazin-1-yl)-ethyl]amine)(azide)4

Base Information

• Chemical Name: Pb₂(N-((1-pyridin-2-yl)benzylidene)-N'-[2-(4-[2-[((1-pyridin-2-yl)benzylidene)amino]ethyl]piperazin-1-yl)-ethyl]amine)(azide)4
• CAS No.: 1220187-94-9
• Molecular Formula: C₃₂H₃₄N₁₈Pb₂
• Molecular Weight: 1085.14
• Mol file: 1220187-94-9.mol

Synonyms:

Chemical Property of Pb₂(N-((1-pyridin-2-yl)benzylidene)-N'-[2-(4-[2-[((1-pyridin-2-yl)benzylidene)amino]ethyl]piperazin-1-yl)-ethyl]amine)(azide)4

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Pb₂(N-((1-pyridin-2-yl)benzylidene)-N'-[2-(4-[2-[((1-pyridin-2-yl)benzylidene)amino]ethyl]piperazin-1-yl)-ethyl]amine)(azide)4

There total 1 articles about Pb₂(N-((1-pyridin-2-yl)benzylidene)-N'-[2-(4-[2-[((1-pyridin-2-yl)benzylidene)amino]ethyl]piperazin-1-yl)-ethyl]amine)(azide)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

sodium azide + N-((1-pyridin-2-yl)benzylidene)-N'-[2-(4-[2-[((1-pyridin-2-yl)benzylidene)amino]ethyl]piperazin-1-yl)-ethyl]amine (959850-48-7) + lead(II) acetate trihydrate (6080-56-4) → Pb2(N-((1-pyridin-2-yl)benzylidene)-N'-[2-(4-[2-[((1-pyridin-2-yl)benzylidene)amino]ethyl]piperazin-1-yl)-ethyl]amine)(azide)4 (1220187-94-9)

Guidance literature:

In methanol; soln. of ligand in MeOH added dropwise to soln. of Pb(CH3CO2)2*3H2O in MeOH, soln. of NaN3 in MeOH added; soln. filtered, filtrate allowed to evap. in air for a few d, crystals filtered off, washed with toluene, dried under vac. over silica; elem. anal.;

DOI:10.1016/j.molstruc.2009.12.015

upstream raw materials:

N-((1-pyridin-2-yl)benzylidene)-N'-[2-(4-[2-[((1-pyridin-2-yl)benzylidene)amino]ethyl]piperazin-1-yl)-ethyl]amine

lead(II) acetate trihydrate

Refernces