Pt₂Br(P(C₆H₅)3)3(SCH₂C(O)C₆H₅)(SCH₂CH₂CH₂CH₃)⁽¹⁺⁾*PF₆^(1-)=[Pt₂Br(P(C₆H₅)3)3(SCH₂C(O)C₆H₅)(SC₄H₉)]PF₆

Base Information

• Chemical Name: Pt₂Br(P(C₆H₅)3)3(SCH₂C(O)C₆H₅)(SCH₂CH₂CH₂CH₃)⁽¹⁺⁾*PF₆^(1-)=[Pt₂Br(P(C₆H₅)3)3(SCH₂C(O)C₆H₅)(SC₄H₉)]PF₆
• CAS No.: 1338071-31-0
• Molecular Formula: C₆₆H₆₁BrOP₃Pt₂S₂*F₆P
• Molecular Weight: 1642.29

Synonyms:

Chemical Property of Pt₂Br(P(C₆H₅)3)3(SCH₂C(O)C₆H₅)(SCH₂CH₂CH₂CH₃)⁽¹⁺⁾*PF₆^(1-)=[Pt₂Br(P(C₆H₅)3)3(SCH₂C(O)C₆H₅)(SC₄H₉)]PF₆

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Technology Process of Pt₂Br(P(C₆H₅)3)3(SCH₂C(O)C₆H₅)(SCH₂CH₂CH₂CH₃)⁽¹⁺⁾*PF₆^(1-)=[Pt₂Br(P(C₆H₅)3)3(SCH₂C(O)C₆H₅)(SC₄H₉)]PF₆

There total 1 articles about Pt₂Br(P(C₆H₅)3)3(SCH₂C(O)C₆H₅)(SCH₂CH₂CH₂CH₃)⁽¹⁺⁾*PF₆^(1-)=[Pt₂Br(P(C₆H₅)3)3(SCH₂C(O)C₆H₅)(SC₄H₉)]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

1-bromo-butane (109-65-9) + ammonium hexafluorophosphate + di-μ-sulphido-tetrakis(triphenylphosphine)-diplatinum(II) + α-bromoacetophenone (70-11-1) → Pt2Br(P(C6H5)3)3(SCH2C(O)C6H5)(SCH2CH2CH2CH3)(1+)*PF6(1-)=[Pt2Br(P(C6H5)3)3(SCH2C(O)C6H5)(SC4H9)]PF6 (1338071-31-0)

Guidance literature:

In methanol; 1-bromobutane (large excess) added to suspn. of Pt compd. in MeOH under stirring, mixt. stirred for 1 h, evapn. under vac., residue dissolved inMeOH, phenacetyl bromide added, soln. stirred for 48 h, soln. filtered, NH4PF6 added to filtrate; water added, ppt. filtered off, washed with water and Et2O, dried under vac.; elem. anal.;

DOI:10.1016/j.ica.2011.06.023

upstream raw materials:

1-bromo-butane

α-bromoacetophenone

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