RuHCl(C₇H₈)(P(C₆H₅)3)2

Base Information

Chemical Name:RuHCl(C₇H₈)(P(C₆H₅)3)2
CAS No.:12392-83-5
Molecular Formula:C₄₃H₃₉ClP₂Ru
Molecular Weight:754.253
Hs Code.:

RuHCl(C<sub>7</sub>H<sub>8</sub>)(P(C<sub>6</sub>H<sub>5</sub>)3)2

Synonyms:

Suppliers and Price of RuHCl(C₇H₈)(P(C₆H₅)3)2

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of RuHCl(C₇H₈)(P(C₆H₅)3)2

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of RuHCl(C₇H₈)(P(C₆H₅)3)2

There total 1 articles about RuHCl(C₇H₈)(P(C₆H₅)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22493-02-3,51383-67-6
{RuHCl(triphenylphosphine)3} * benzene

: 121-46-0
bicyclo[2.2.1]hepta-2,5-diene

: 12392-83-5
{RuHCl(norbornadiene)(triphenylphosphine)2}

Guidance literature:

Reference yield: 88.3%

: 12392-83-5,89395-73-3
RuHCl(C₇H₈)(P(C₆H₅)3)2

: 1493-13-6
trifluorormethanesulfonic acid

: Ru₃Cl₅(P(C₆H₅)3)6⁽¹⁺⁾*CF₃SO₃^(1-)=Ru₃Cl₅(P(C₆H₅)3)6CF₃SO₃

Guidance literature:: In dichloromethane; water; mixt. of Ru-complex and ligand in CH2Cl2 and water was stirred for 72 h under N2; aq. layer was removed, CH2Cl2 layer was washed with water, solvent was removed under vac., Et2O was added, stirred for 20 min, dried under vac.;elem. anal.;
DOI:10.1021/om010029r

Reference yield: 60.0%

: 12392-83-5,89395-73-3
RuHCl(C₇H₈)(P(C₆H₅)3)2

: 2923-28-6
silver trifluoromethanesulfonate

: 308366-36-1
[RuH(OSO₂CF₃)(C₇H₈)(P(C₆H₅)3)2]

Guidance literature:: In tetrahydrofuran; (N2); standard Schlenk technique; mixt. of Ru complex and AgOTf in THF stirred for 0.5 h; solvent removed in vac.; aq. MeOH added; filtered; washed (water); dried in vac. for 3 h; extd. (benzene/hexane, 8/1); filtered through Celite column; concd.; hexane added; filtered; washed (hexane); dried (vac.); elem. anal.;
DOI:10.1021/om000369x