p-chloromercuri{2-⁽³⁾H}toluene

Base Information

Chemical Name:p-chloromercuri{2-⁽³⁾H}toluene
CAS No.:142414-88-8
Molecular Formula:C₇H₇ClHg
Molecular Weight:329.168
Hs Code.:

p-chloromercuri{2-<sup>(3)</sup>H}toluene

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-chloromercuri{2-⁽³⁾H}toluene

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Technology Process of p-chloromercuri{2-⁽³⁾H}toluene

There total 1 articles about p-chloromercuri{2-⁽³⁾H}toluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54615-78-0
{2-(3)H}toluene

: 7647-14-5
sodium chloride

: 12653-71-3
mercury(II) oxide

: 142414-88-8
p-chloromercuri{2-⁽³⁾H}toluene

Guidance literature:: In perchloric acid; acetic acid; stirring (3)H-labelled toluene (from o-bromotoluene and (3)H2) and HgO in glacial acetic acid and 30% HClO4 for 6h, removal of acetic acid and excess of (3)H-labelled toluene, addn. of 1M NaCl-soln. to the residue, pptn.;; cooling to -3°C for 3h, centrifugation, washing with H2O, drying in a rotary evaporator;;

Reference yield: 50.0%

: 142414-88-8
p-chloromercuri{2-⁽³⁾H}toluene

: 142414-89-9
p-chloromercuri{2-⁽³⁾H}benzoic acid

Guidance literature:: With potassium permanganate; In sodium hydroxide; byproducts: MnO2; heating a mixture of 10-20mg Hg-compound, 0.6ml 1M NaOH and 18-27mg KMnO4 on a water bath for 1.5h, addn. of 2-4 drops of ethanol to destroy excess KMnO4;; separation of MnO2, pptn. on addn. of concd. HCl, cooling to 5°C for 2h, centrifugation, washing with H2O, drying in a rotary evaporator; purification by preparative TLC (NH3-soln. on silica gel, ethylacetate/ethanol/NH3=1:1:2);;