(+/-)-1-(4-chlorophenyl)-2-thiocyanatoethyl acetate

Base Information

Chemical Name:(+/-)-1-(4-chlorophenyl)-2-thiocyanatoethyl acetate
CAS No.:70372-46-2
Molecular Formula:C₁₁H₁₀ClNO₂S
Molecular Weight:255.725
Hs Code.:

Synonyms:

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Chemical Property of (+/-)-1-(4-chlorophenyl)-2-thiocyanatoethyl acetate

Chemical Property:

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Technology Process of (+/-)-1-(4-chlorophenyl)-2-thiocyanatoethyl acetate

There total 4 articles about (+/-)-1-(4-chlorophenyl)-2-thiocyanatoethyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2788-86-5
4-Chlorostyrene oxide

: 1147550-11-5
ammonium thiocyanate

: 75-36-5
acetyl chloride

: 70372-46-2
(+/-)-1-(4-chlorophenyl)-2-thiocyanatoethyl acetate

: 1-(4-chlorophenyl)-2-hydroxyethyl thiocyanate

Guidance literature:: 4-Chlorostyrene oxide; ammonium thiocyanate; With 18-crown-6 ether; In dichloromethane; acetonitrile; Heating;

acetyl chloride; for 2.5h; Heating;

With phosphate buffer; immobilized Novozym SP 435; at 17 - 20 ℃; pH=7;
DOI:10.1016/j.tetasy.2005.05.007

Reference yield:

: 2788-86-5
4-Chlorostyrene oxide

: 1147550-11-5
ammonium thiocyanate

: 75-36-5
acetyl chloride

: 70372-46-2
(+/-)-1-(4-chlorophenyl)-2-thiocyanatoethyl acetate

: acetic acid 2-(4-chloro-phenyl)-2-thiocyanato-ethyl ester

Guidance literature:: 4-Chlorostyrene oxide; ammonium thiocyanate; With 18-crown-6 ether; In dichloromethane; acetonitrile; Heating;

acetyl chloride; for 2.5h; Title compound not separated from byproducts; Heating;
DOI:10.1016/j.tetasy.2005.05.007