(CuBr)3(tris(2-(3-phenylpropylthio)ethyl)triazacyclohexane)

Base Information

Chemical Name:(CuBr)3(tris(2-(3-phenylpropylthio)ethyl)triazacyclohexane)
CAS No.:1174513-02-0
Molecular Formula:C₃₆H₅₁Br₃Cu₃N₃S₃
Molecular Weight:1052.37
Hs Code.:

Synonyms:

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Chemical Property of (CuBr)3(tris(2-(3-phenylpropylthio)ethyl)triazacyclohexane)

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Technology Process of (CuBr)3(tris(2-(3-phenylpropylthio)ethyl)triazacyclohexane)

There total 1 articles about (CuBr)3(tris(2-(3-phenylpropylthio)ethyl)triazacyclohexane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1174512-91-4
tris(2-(3-phenylpropylthio)ethyl)triazacyclohexane

: 7787-70-4
copper(I) bromide

: 1174513-02-0
(CuBr)3(tris(2-(3-phenylpropylthio)ethyl)triazacyclohexane)

Guidance literature:: In acetonitrile; (under Ar or N2, Schlenk); ligand dissolved in MeCN, added to CuBr, stirred overnight; decanted, washed with Et2O, dried in vacuo; elem. anal.;
DOI:10.1039/b819268e

Reference yield: 71.0%

: 1174513-02-0
(CuBr)3(tris(2-(3-phenylpropylthio)ethyl)triazacyclohexane)

: 7681-82-5,24359-64-6,41927-88-2,115813-40-6
sodium iodide

: 1174513-03-1
(CuI)3(tris(2-(3-phenylpropylthio)ethyl)triazacyclohexane)

Guidance literature:: In dichloromethane; water; (under Ar or N2, Schlenk); aq. soln. of NaI added to CH2Cl2 soln. of Cu-complex, stirred for 1 h; organic phase collected, solvent evapd. under vac.; elem. anal.;
DOI:10.1039/b819268e

Reference yield: 62.0%

: 1174513-02-0
(CuBr)3(tris(2-(3-phenylpropylthio)ethyl)triazacyclohexane)

: 7647-14-5
sodium chloride

: 1174513-01-9
(CuCl)3(tris(2-(3-phenylpropylthio)ethyl)triazacyclohexane)

Guidance literature:: With AgNO₃; In dichloromethane; water; byproducts: AgCl; (under Ar or N2, Schlenk); CH2Cl2 soln. of Cu-complex added to satd. soln. of NaCl in H2O, AgNO3 added, stirred for 2 h; organic phase collected, solvent evapd.;
DOI:10.1039/b819268e