C₃₀H₃₆O₅Se

Base Information

Chemical Name:C₃₀H₃₆O₅Se
CAS No.:88509-19-7
Molecular Formula:C₃₀H₃₆O₅Se
Molecular Weight:555.573
Hs Code.:

C<sub>30</sub>H<sub>36</sub>O<sub>5</sub>Se

Synonyms:

Suppliers and Price of C₃₀H₃₆O₅Se

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₀H₃₆O₅Se

Chemical Property:

Purity/Quality:

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Technology Process of C₃₀H₃₆O₅Se

There total 1 articles about C₃₀H₃₆O₅Se which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5707-04-0
Phenylselenyl chloride

: 80163-63-9,88509-13-1,88548-10-1
16α-methyl-17α,20;20,21-bismethylenedioxy-pregn-4,9(11)-diene-3-one

: 88509-18-6,88509-19-7
C₃₀H₃₆O₅Se

Guidance literature:: With lithium diisopropyl amide; Multistep reaction; 1.) THF, -78 deg C, 1 h then 0 deg C, 5 h; 2.) THF, -78 deg C, 3.5 h;
DOI:10.1016/S0040-4020(01)91549-2

Reference yield:

: 88509-18-6,88509-19-7
C₃₀H₃₆O₅Se

: 50-02-2
dexamethasone

Guidance literature:: Multi-step reaction with 4 steps

1: 63 percent / sodium metaperiodate / tetrahydrofuran; methanol; H₂O / 2.5 h / Ambient temperature

2: 95 percent / 0.4M perchloric acid, N-bromoacetamide / dioxane / 15 h / Ambient temperature

3: 87 percent / potassium acetate / ethanol; dioxane / 19 h / Heating

4: 48percent hydrofluoric acid / ethanol; tetrahydrofuran / 20 h / 0 °C

With sodium periodate; perchloric acid; hydrogen fluoride; potassium acetate; N-bromoacetamide; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; water;
DOI:10.1016/S0040-4020(01)91549-2

Reference yield:

: 88509-18-6,88509-19-7
C₃₀H₃₆O₅Se

: C₂₇⁽¹³⁾C₃H₃₆O₅Se

Guidance literature:: Multi-step reaction with 14 steps

1: 63 percent / sodium metaperiodate / tetrahydrofuran; methanol; H₂O / 2.5 h / Ambient temperature

2: Zn / dimethylformamide; H₂O / 145-147 deg C, 30 min; room temp., 2 h

3: 48 percent / Bu₄NHSO₄, NaOH / tetrahydrofuran; H₂O / 5-10 deg C, 0.5 h, then room temp., 16 h

4: NH₃, Li / tetrahydrofuran / 2 h / -78 °C

5: NH₃, Li / tetrahydrofuran; ethanol

6: 1M oxalic acid / tetrahydrofuran; methanol / 2.5 h

7: 50 percent / pyridinium bromide perbromide / pyridine / room temp., 2 h 85 deg C, 1 h

8: 1.) O₃; 2.) H₂O₂ / 1.) CH₂Cl₂, MeOH, acetic acid, -72 deg C, 3.5 h; 2.) water, room temp., 18 h

9: NaOAc / acetic anhydride / 2.5 h / 100 °C

10: 1.) n-BuLi / 1.) THF, -78 deg C, 50 min; 2.) THF, -78 deg C, 4 h, then room temp., 15 h

11: sodium t-amyloxide / toluene / 0.67 h / Heating

12: 75 percent / glacial AcOH / H₂O / 1.25 h / 65 °C

13: 82 percent / KO(t-butyl) / 2-methyl-propan-2-ol / 17 h / Ambient temperature

14: LDA / tetrahydrofuran

With sodium hydroxide; sodium periodate; n-butyllithium; potassium tert-butylate; ammonia; dihydrogen peroxide; sodium acetate; tetra(n-butyl)ammonium hydrogensulfate; pyridinium hydrobromide perbromide; oxalic acid; lithium; sodium tert-pentoxide; ozone; acetic acid; zinc; lithium diisopropyl amide; In tetrahydrofuran; pyridine; methanol; ethanol; water; acetic anhydride; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;
DOI:10.1016/S0040-4020(01)91549-2