[RuCl(η6-p-MeC6H4(i)Pr)(1-diphenylphosphinoaminopiperidine)][BF4]

Base Information

Chemical Name:[RuCl(η6-p-MeC6H4(i)Pr)(1-diphenylphosphinoaminopiperidine)][BF4]
CAS No.:849371-40-0
Molecular Formula:BF₄*C₂₇H₃₅ClN₂PRu
Molecular Weight:641.89
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [RuCl(η6-p-MeC6H4(i)Pr)(1-diphenylphosphinoaminopiperidine)][BF4]

Chemical Property:

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Technology Process of [RuCl(η6-p-MeC6H4(i)Pr)(1-diphenylphosphinoaminopiperidine)][BF4]

There total 1 articles about [RuCl(η6-p-MeC6H4(i)Pr)(1-diphenylphosphinoaminopiperidine)][BF4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 14104-20-2
silver tetrafluoroborate

: 849371-44-4
[RuCl2(η6-p-MeC6H4(i)Pr)(1-diphenylphosphinoaminopiperidine)]*CH2Cl2

: 849371-40-0
[RuCl(η6-p-MeC6H4(i)Pr)(1-diphenylphosphinoaminopiperidine)][BF4]

Guidance literature:: In toluene; benzene; byproducts: AgCl; under N2; to a soln. of Ru-contg. compd. (0.34 mmol) in toluene, a benzene soln. of AgBF4 (0.30 mmol) was added in the dark during 5 min; stirring at room temp. for 15 min; the mixt. was left to stand for ca. 1 h; solid was isolated by filtration, washed with toluene, dissolved in CH2Cl2 and left to stand for 10 min; suspn. was filtered and the vol. was reduced under vac.; pentane was added for pptn.; the solid was isolated and dried under vac.; elem. anal.;
DOI:10.1039/b417068g