[PtCl(P,P',N-1,2-bis(di(o-N,N-dimethylanilinyl)phosphino)ethane)]Cl

Base Information

Chemical Name:[PtCl(P,P',N-1,2-bis(di(o-N,N-dimethylanilinyl)phosphino)ethane)]Cl
CAS No.:852636-57-8
Molecular Formula:C₃₄H₄₄ClN₄P₂Pt*Cl
Molecular Weight:836.684
Hs Code.:

Synonyms:

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Chemical Property of [PtCl(P,P',N-1,2-bis(di(o-N,N-dimethylanilinyl)phosphino)ethane)]Cl

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Technology Process of [PtCl(P,P',N-1,2-bis(di(o-N,N-dimethylanilinyl)phosphino)ethane)]Cl

There total 2 articles about [PtCl(P,P',N-1,2-bis(di(o-N,N-dimethylanilinyl)phosphino)ethane)]Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 12080-32-9
dichloro( 1,5-cyclooctadiene)platinum(ll)

: 532390-74-2
1,2-bis(di(o-N,N-dimethylanilinyl)phosphino)ethane

: 852636-57-8,852636-48-7
PtCl₂(P,P'-1,2-bis(di(o-N,N-dimethylanilinyl)phosphino)ethane)

Guidance literature:: In dichloromethane; under inert atm. PtCl2(cod) and ligand in CH2Cl2 were stirred at room temp. for 17 h; solvent was removed in vacuo, residue was dissolved in CH2Cl2, Et2O was added, ppt. was filtered, washed with Et2O and drued in vacuo at 78°C; elem. anal.;
DOI:10.1021/ic048639h

Reference yield: 40.0%

: 75-05-8,26809-02-9
acetonitrile

: 10025-65-7
platinum(II) chloride

: 532390-74-2
1,2-bis(di(o-N,N-dimethylanilinyl)phosphino)ethane

: 852636-57-8,852636-48-7
PtCl₂(P,P'-1,2-bis(di(o-N,N-dimethylanilinyl)phosphino)ethane)

Guidance literature:: In acetonitrile; under inert atm. slurry PtCl2 in MeCN was refluxed for 2 h, ligand was added to hot soln.; solvent was removed in vacuo, residue was dissolved in CH2Cl2, Et2O was added, ppt. was filtered, washed with Et2O and drued in vacuo at 78°C;
DOI:10.1021/ic048639h

Reference yield: 47.0%

: ammonium hexafluorophosphate

: 852636-57-8,852636-48-7
[PtCl(P,P',N-1,2-bis(di(o-N,N-dimethylanilinyl)phosphino)ethane)]Cl

: 852636-50-1
[PtCl(P,P',N-1,2-bis(di(o-N,N-dimethylanilinyl)phosphino)ethane)]PF₆

Guidance literature:: In acetone; under inert atm. Pt complex and NH4PF6 in acetone was stirred at room temp. (20°C) for 1 h; solvent was removed, residue was taken up in CH2Cl2 and was filtered through Celite; elem. anal.;
DOI:10.1021/ic048639h