(-)-(2R)-2-Methyl-2-phenylbutanoyl chloride

Base Information

Chemical Name:(-)-(2R)-2-Methyl-2-phenylbutanoyl chloride
CAS No.:157750-19-1
Molecular Formula:C₁₁H₁₃ClO
Molecular Weight:196.677
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (-)-(2R)-2-Methyl-2-phenylbutanoyl chloride

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Technology Process of (-)-(2R)-2-Methyl-2-phenylbutanoyl chloride

There total 3 articles about (-)-(2R)-2-Methyl-2-phenylbutanoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 3968-67-0
(-)-(2R)-2-Methyl-2-phenylbutanoic acid

: 157750-19-1
(-)-(2R)-2-Methyl-2-phenylbutanoyl chloride

Guidance literature:: With thionyl chloride; for 20h;
DOI:10.1002/recl.19941130602

Reference yield:

: 5558-93-0
(+/-)-2-methyl-2-phenyl-butyronitrile

: 157750-19-1
(-)-(2R)-2-Methyl-2-phenylbutanoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: KOH / bis-(2-hydroxy-ethyl) ether / 24 h / Heating

2: 95 percent / SOCl₂ / 20 h

With potassium hydroxide; thionyl chloride; In diethylene glycol;
DOI:10.1002/recl.19941130602

Reference yield:

: 769-68-6
2-phenylbutanenitrile

: 157750-19-1
(-)-(2R)-2-Methyl-2-phenylbutanoyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: diisopropylamine, BuLi / tetrahydrofuran; hexane / 1.) -20 deg C, 4 h, 2.) 0 deg C, 2 h

2: KOH / bis-(2-hydroxy-ethyl) ether / 24 h / Heating

3: 95 percent / SOCl₂ / 20 h

With potassium hydroxide; n-butyllithium; thionyl chloride; diisopropylamine; In tetrahydrofuran; hexane; diethylene glycol;
DOI:10.1002/recl.19941130602