4-chlorobutyl(phenyl)phosphinothioic chloride

Base Information

Chemical Name:4-chlorobutyl(phenyl)phosphinothioic chloride
CAS No.:231610-98-3
Molecular Formula:C₁₀H₁₃Cl₂PS
Molecular Weight:267.159
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-chlorobutyl(phenyl)phosphinothioic chloride

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Technology Process of 4-chlorobutyl(phenyl)phosphinothioic chloride

There total 5 articles about 4-chlorobutyl(phenyl)phosphinothioic chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 231610-97-2
C₁₀H₁₃Cl₂OP

: 231610-98-3
4-chlorobutyl(phenyl)phosphinothioic chloride

Guidance literature:: With tetraphosphorus decasulfide; N,N-dimethyl-formamide; In 1,4-dioxane; for 2h; Heating;
DOI:10.1039/a900623k

Reference yield:

: 1638-86-4
diethyl phenylphosphonite

: 231610-98-3
4-chlorobutyl(phenyl)phosphinothioic chloride

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / Heating

2: 31 percent / HCl, H₂O / 4.5 h / Heating

3: oxalyl chloride / CH₂Cl₂ / 0.5 h

4: P₄S₁₀, DMF / dioxane / 2 h / Heating

With hydrogenchloride; tetraphosphorus decasulfide; oxalyl dichloride; water; N,N-dimethyl-formamide; In 1,4-dioxane; dichloromethane;
DOI:10.1039/a900623k

Reference yield:

: 644-97-3
Dichlorophenylphosphine

: 231610-98-3
4-chlorobutyl(phenyl)phosphinothioic chloride

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / light petroleum

2: 70 percent / Heating

3: 31 percent / HCl, H₂O / 4.5 h / Heating

4: oxalyl chloride / CH₂Cl₂ / 0.5 h

5: P₄S₁₀, DMF / dioxane / 2 h / Heating

With pyridine; hydrogenchloride; tetraphosphorus decasulfide; oxalyl dichloride; water; N,N-dimethyl-formamide; In 1,4-dioxane; dichloromethane; Petroleum ether;
DOI:10.1039/a900623k