trans-4,4'-bisazobenzene

Base Information

• Chemical Name: trans-4,4'-bisazobenzene
• CAS No.: 79951-06-7
• Molecular Formula: C₂₂H₂₄N₄O₈
• Molecular Weight: 472.455

Synonyms:

Chemical Property of trans-4,4'-bisazobenzene

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of trans-4,4'-bisazobenzene

There total 2 articles about trans-4,4'-bisazobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

(E)-4,4'-bis(chloromethyl)azobenzene (99833-18-8) + iminodiacetic acid (142-73-4) → trans-4,4'-bisazobenzene (79951-06-7)

Guidance literature:

With potassium carbonate; In methanol; water; for 21h; Heating;

DOI:10.1246/bcsj.58.2340

Reference yield:

[(4-{4-[(Bis-carboxymethyl-amino)-methyl]-phenylazo}-benzyl)-carboxymethyl-amino]-acetic acid → trans-4,4'-bisazobenzene (79951-06-7)

Guidance literature:

at 30 ℃; Rate constant; pH 9.02, NH₃ buffer, influence of Zn(II) and Cu(II);

DOI:10.1246/bcsj.58.2340

Reference yield:

trans-4,4'-bisazobenzene (79951-06-7) → [(4-{4-[(Bis-carboxymethyl-amino)-methyl]-phenylazo}-benzyl)-carboxymethyl-amino]-acetic acid

Guidance literature:

for 0.0833333h; Product distribution; Irradiation; Hg-lamp (filtered to 330-380 nm);

DOI:10.1246/bcsj.58.2340

upstream raw materials:

(E)-4,4'-bis(chloromethyl)azobenzene

iminodiacetic acid

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