4-(1,3-Dioxolan-2-yl)-4-methylcyclohex-2-en-1-one

Base Information

Chemical Name:4-(1,3-Dioxolan-2-yl)-4-methylcyclohex-2-en-1-one
CAS No.:114300-65-1
Molecular Formula:C10H14O3
Molecular Weight:182.219
Hs Code.:
DSSTox Substance ID:DTXSID20555365
Nikkaji Number:J1.662.717H
Mol file:114300-65-1.mol

Synonyms:114300-65-1;4-(1,3-Dioxolan-2-yl)-4-methylcyclohex-2-en-1-one;DTXSID20555365

Suppliers and Price of 4-(1,3-Dioxolan-2-yl)-4-methylcyclohex-2-en-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(1,3-Dioxolan-2-yl)-4-methylcyclohex-2-en-1-one

Chemical Property:

XLogP3:0.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:182.094294304
Heavy Atom Count:13
Complexity:241

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(CCC(=O)C=C1)C2OCCO2

Technology Process of 4-(1,3-Dioxolan-2-yl)-4-methylcyclohex-2-en-1-one

There total 1 articles about 4-(1,3-Dioxolan-2-yl)-4-methylcyclohex-2-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54125-08-5
4-methyl-4-formylcyclohex-2-enone

: 107-21-1
ethylene glycol

: 114300-65-1
4-[1,3]Dioxolan-2-yl-4-methyl-cyclohex-2-enone

Guidance literature:: With copper dichloride; In benzene;
DOI:10.1016/S0040-4039(01)02139-6

Reference yield: 84.0%

: 17640-15-2
methyl cyanoformate

: 114300-65-1
4-[1,3]Dioxolan-2-yl-4-methyl-cyclohex-2-enone

: 5-[1,3]dioxolan-2-yl-2-hydroxy-5-methyl-cyclohexa-1,3-dienecarboxylic acid methyl ester

Guidance literature:: With lithium hexamethyldisilazane; In N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1016/S0040-4039(01)02139-6

Reference yield:

: 814-49-3
diethyl chlorophosphate

: 114300-65-1
4-[1,3]Dioxolan-2-yl-4-methyl-cyclohex-2-enone

: 137626-82-5
Phosphoric acid 4-[1,3]dioxolan-2-yl-4-methyl-cyclohexa-1,5-dienyl ester diethyl ester

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction; 1a) THF, -75 to 0 deg C, 2 h, 1b) 0 deg C, 1 h, 2) -75 deg C, 4 h;
DOI:10.1021/jo00027a055