Technology Process of C26H29F3O4
There total 7 articles about C26H29F3O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap; dicyclohexyl-carbodiimide;
In
dichloromethane;
at 20 ℃;
Inert atmosphere;
DOI:10.1002/anie.201208132
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydride / tetrahydrofuran / 0 °C / Inert atmosphere
2: disodium ethylenediaminetetraacetic acid; potassium carbonate; Oxone; borax; tetra(n-butyl)ammonium hydrogensulfate / water; acetonitrile / 0 °C / Inert atmosphere
3: diisobutylaluminium hydride / dichloromethane / -78 °C / Inert atmosphere
4: perrhenic acid anhydride / dichloromethane / 0.75 h / 20 °C / Inert atmosphere
5: dicyclohexyl-carbodiimide; dmap / dichloromethane / 20 °C / Inert atmosphere
With
dmap; borax; Oxone; perrhenic acid anhydride; tetra(n-butyl)ammonium hydrogensulfate; disodium ethylenediaminetetraacetic acid; sodium hydride; diisobutylaluminium hydride; potassium carbonate; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; dichloromethane; water; acetonitrile;
DOI:10.1002/anie.201208132
- Guidance literature:
-
Multi-step reaction with 2 steps
1: perrhenic acid anhydride / dichloromethane / 0.75 h / 20 °C / Inert atmosphere
2: dicyclohexyl-carbodiimide; dmap / dichloromethane / 20 °C / Inert atmosphere
With
dmap; perrhenic acid anhydride; dicyclohexyl-carbodiimide;
In
dichloromethane;
DOI:10.1002/anie.201208132
