methyl 4²-O-benzoyl-α-L-pillaroside

Base Information

Chemical Name:methyl 4²-O-benzoyl-α-L-pillaroside
CAS No.:59531-21-4
Molecular Formula:C₁₆H₂₀O₆
Molecular Weight:308.331
Hs Code.:

methyl 4<sup>2</sup>-O-benzoyl-α-L-pillaroside

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Chemical Property of methyl 4²-O-benzoyl-α-L-pillaroside

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Technology Process of methyl 4²-O-benzoyl-α-L-pillaroside

There total 7 articles about methyl 4²-O-benzoyl-α-L-pillaroside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 98-88-4
benzoyl chloride

: 67772-71-8
methyl α-L-pillaroside

: 59531-21-4
methyl 4²-O-benzoyl-α-L-pillaroside

Guidance literature:: With pyridine; Ambient temperature;

Reference yield:

: 40246-38-6
methyl-2,3,6-tridesoxy-α-L-erythro-hex-2-enopyranoside

: 59531-21-4
methyl 4²-O-benzoyl-α-L-pillaroside

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / manganese dioxide / CHCl₃ / Ambient temperature

2: 76 percent / hydrogen / palladium-charcoal / methanol

3: tetrahydrofuran; pentane / 1.) -60 deg C, 30 min, 2.) -60 --> 0 deg C, 30 min

4: 30 percent / m-chloroperbenzoic acid, water / diethyl ether / 2 h / Ambient temperature

5: 75 percent / pyridine / Ambient temperature

With pyridine; manganese(IV) oxide; water; hydrogen; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; chloroform; pentane;

Reference yield:

: 55102-46-0
methyl 2,3,6-trideoxy-α-L-glycero-hex-2-enopyranosid-4-ulose

: 59531-21-4
methyl 4²-O-benzoyl-α-L-pillaroside

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / hydrogen / palladium-charcoal / methanol

2: tetrahydrofuran; pentane / 1.) -60 deg C, 30 min, 2.) -60 --> 0 deg C, 30 min

3: 30 percent / m-chloroperbenzoic acid, water / diethyl ether / 2 h / Ambient temperature

4: 75 percent / pyridine / Ambient temperature

With pyridine; water; hydrogen; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; pentane;