diphenyltin(IV) p-chlorobenzohydroxamate * acetylacetonate

Base Information

• Chemical Name: diphenyltin(IV) p-chlorobenzohydroxamate * acetylacetonate
• CAS No.: 198631-11-7
• Molecular Formula: C₂₄H₂₂ClNO₄Sn
• Molecular Weight: 542.606
• Mol file: 198631-11-7.mol

Synonyms:

Chemical Property of diphenyltin(IV) p-chlorobenzohydroxamate * acetylacetonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of diphenyltin(IV) p-chlorobenzohydroxamate * acetylacetonate

There total 3 articles about diphenyltin(IV) p-chlorobenzohydroxamate * acetylacetonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

diphenylmonochlorotin(IV) p-chlorobenzohydroxamate (198630-99-8) + sodium (Z)-4-oxopent-2-en-2-olate (1118-67-8) → diphenyltin(IV) p-chlorobenzohydroxamate * acetylacetonate (198631-11-7)

Guidance literature:

In methanol; byproducts: NaCl; stirring (room temp.), refluxing (6 - 8 h); filtration, concn. of filtrate, sepn., washing (petroleum ether), recrystn. (MeOH); elem. anal.;

DOI:10.1080/00945719708000166

Reference yield:

potassium p-chlorobenzohydroxyamate (57139-20-5) → diphenyltin(IV) p-chlorobenzohydroxamate * acetylacetonate (198631-11-7)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran; methanol

2: methanol

In tetrahydrofuran; methanol;

DOI:10.1080/00945719708000166

Reference yield:

diphenyltin(IV) dichloride (1135-99-5) → diphenyltin(IV) p-chlorobenzohydroxamate * acetylacetonate (198631-11-7)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran; methanol

2: methanol

In tetrahydrofuran; methanol;

DOI:10.1080/00945719708000166

upstream raw materials:

diphenylmonochlorotin(IV) p-chlorobenzohydroxamate

sodium (Z)-4-oxopent-2-en-2-olate

potassium p-chlorobenzohydroxyamate

diphenyltin(IV) dichloride