3-cyano-6-methoxy-4-oxo-1,4-dihydroquinolin-7-yl trifluoromethanesulfonate

Base Information

Chemical Name:3-cyano-6-methoxy-4-oxo-1,4-dihydroquinolin-7-yl trifluoromethanesulfonate
CAS No.:364793-71-5
Molecular Formula:C₁₂H₇F₃N₂O₅S
Molecular Weight:348.259
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-cyano-6-methoxy-4-oxo-1,4-dihydroquinolin-7-yl trifluoromethanesulfonate

Chemical Property:

Vapor Pressure:0mmHg at 25°C

Purity/Quality:

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Technology Process of 3-cyano-6-methoxy-4-oxo-1,4-dihydroquinolin-7-yl trifluoromethanesulfonate

There total 7 articles about 3-cyano-6-methoxy-4-oxo-1,4-dihydroquinolin-7-yl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65-85-0,8013-63-6
benzoic acid

: 364793-71-5
3-cyano-6-methoxy-4-oxo-1,4-dihydro-7-quinolinyl trifluoromethanesulfonate

Guidance literature:: With n-butyllithium; acetic acid; In tetrahydrofuran; hexane; water; ethyl acetate; acetonitrile;

Reference yield:

: 3943-74-6
4-hydroxy-3-methoxybenzoic acid methyl ester

: 364793-71-5
3-cyano-6-methoxy-4-oxo-1,4-dihydro-7-quinolinyl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 6 steps

1.1: K₂CO₃ / dimethylformamide

2.1: HNO₃; AcOH

3.1: BCl₃ / CH₂Cl₂

4.1: pyridine / CH₂Cl₂

5.1: Fe; aq. NH₄Cl / methanol

6.2: nBuLi / tetrahydrofuran

With pyridine; nitric acid; boron trichloride; iron; potassium carbonate; ammonium chloride; acetic acid; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(02)00577-2

Reference yield:

: 61032-41-5
methyl 4-(benzyloxy)-5-methoxy-2-nitrobenzoate

: 364793-71-5
3-cyano-6-methoxy-4-oxo-1,4-dihydro-7-quinolinyl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: BCl₃ / CH₂Cl₂

2.1: pyridine / CH₂Cl₂

3.1: Fe; aq. NH₄Cl / methanol

4.2: nBuLi / tetrahydrofuran

With pyridine; boron trichloride; iron; ammonium chloride; In methanol; dichloromethane;
DOI:10.1016/S0960-894X(02)00577-2