((C₆H₅)3PAu)3Mn(CO)4

Base Information

Chemical Name:((C₆H₅)3PAu)3Mn(CO)4
CAS No.:156429-18-4
Molecular Formula:C₅₈H₄₅Au₃MnO₄P₃
Molecular Weight:1544.75
Hs Code.:

((C<sub>6</sub>H<sub>5</sub>)3PAu)3Mn(CO)4

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Chemical Property of ((C₆H₅)3PAu)3Mn(CO)4

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Technology Process of ((C₆H₅)3PAu)3Mn(CO)4

There total 4 articles about ((C₆H₅)3PAu)3Mn(CO)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.6%

: 20224-83-3
PPh₃Au^IC₈H₅

: 14692-78-5
{(C₆H₅)3PAuMn(CO)5}

: 24169-91-3
isocyanato(triphenylphosphine)gold(I)

: 156429-18-4,59030-43-2
((C₆H₅)3PAu)3Mn(CO)4

Guidance literature:: In tetrahydrofuran; Irradiation (UV/VIS); dissolving Ph3PAuMn(CO)5 (0.38 mmol), Ph3PAuNCO (0.38 mmol) and Ph3PAuN3 (0.12 mmmol) in freshly distd. THF; irradiation for 30 min with high-pressure-Hg-lamp;; evapn. to dryness; taking up residue in CH2Cl2, filtering; column chromy. (Al2O3, THF); elem. anal.;;

Reference yield: 50.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 10170-69-1
dimanganese decacarbonyl

: Au₈(PPh₃)8(NO₃)2

: 156429-18-4,59030-43-2
((C₆H₅)3PAu)3Mn(CO)4

: ((C₆H₅)3PAu)4[AuMn(CO)5]2*C₄H₈O

Guidance literature:: With KB[CH(CH₃)C₂H₅]3H; In tetrahydrofuran; Soln. of K compd. added to soln. of carbonyl compd. with stirring, after 30 min mixt. added to suspn. of Au complex in THF, stirred for 2 h at room temp.; filtered, n-hexane added to filtrate, allowed to stand in refrigerator for 1 d, filtered, washed with n-hexane, dried in vac., washed with toluene, dissolved in THF, n-hexane layered, crystd. at room temp in dark;
DOI:10.1515/znb-2000-1004

Reference yield:

: 10170-69-1
dimanganese decacarbonyl

: Au₈(PPh₃)8(NO₃)2

: 156429-18-4,59030-43-2
((C₆H₅)3PAu)3Mn(CO)4

: ((C₆H₅)3PAu)4[AuMn(CO)5]2

Guidance literature:: With KB[CH(CH₃)C₂H₅]3H; In tetrahydrofuran; Soln. of K compd. added to soln. of carbonyl compd. with stirring, after 30 min mixt. added to suspn. of Au complex in THF, stirred for 2 h at room temp.; filtered, n-hexane added to filtrate, allowed to stand in refrigerator for 1 d, filtered, washed with n-hexane, dried in vac.;
DOI:10.1515/znb-2000-1004