1,2-Ethanediamine, N,N'-bis(phenyl-2-pyridinylmethylene)-

Base Information

• Chemical Name: 1,2-Ethanediamine, N,N'-bis(phenyl-2-pyridinylmethylene)-
• CAS No.: 115172-00-4
• Molecular Formula: C26H22N4
• Molecular Weight: 390.487
• DSSTox Substance ID: DTXSID30476638
• Nikkaji Number: J1.744.798J
• Mol file: 115172-00-4.mol

Synonyms:1,2-Ethanediamine, N,N'-bis(phenyl-2-pyridinylmethylene)-;115172-00-4;DTXSID30476638

Chemical Property of 1,2-Ethanediamine, N,N'-bis(phenyl-2-pyridinylmethylene)-

Chemical Property:

• XLogP3: 5.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 7
• Exact Mass: 390.18444672
• Heavy Atom Count: 30
• Complexity: 507

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(=NCCN=C(C2=CC=CC=C2)C3=CC=CC=N3)C4=CC=CC=N4

Technology Process of 1,2-Ethanediamine, N,N'-bis(phenyl-2-pyridinylmethylene)-

There total 1 articles about 1,2-Ethanediamine, N,N'-bis(phenyl-2-pyridinylmethylene)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

phenyl(pyridin-2-yl)methanone (91-02-1) + ethylenediamine (107-15-3,85404-18-8) → N,N’-(ethane-1,2-diyl)bis(1-phenyl-1-{pyridin-2-yl}methanimine) (115172-00-4)

Guidance literature:

In methanol; at 20 ℃; for 7h; Reflux;

DOI:10.3184/174751918X15422215897056

Reference yield: 79.0%

Mn(CH3COO)2·H2O (113859-74-8) + N,N’-(ethane-1,2-diyl)bis(1-phenyl-1-{pyridin-2-yl}methanimine) (115172-00-4) → N,N’-(ethane-1,2-diyl)bis(1-phenyl-1-{pyridin-2-yl}methanimine)bisacetatomanganese(II) trihydrate

Guidance literature:

In methanol; at 60 ℃; for 4h;

DOI:10.3184/174751918X15422215897056

Reference yield: 75.0%

piperidinium terephthalate + sodium perchlorate + lead(II) acetate trihydrate (6080-56-4) + N,N’-(ethane-1,2-diyl)bis(1-phenyl-1-{pyridin-2-yl}methanimine) (115172-00-4) → [Pb2(N,N'-(bis(pyridin-2-yl)benzylidene)-1,2-ethanediamine)2(μ-terephthalate)](ClO4)2

Guidance literature:

With air; In methanol; at 20 ℃;

DOI:10.1016/j.molstruc.2013.08.016

upstream raw materials:

phenyl(pyridin-2-yl)methanone

ethylenediamine

Downstream raw materials:

{Co(bis(benzoylpyridine)ethylenediimine)Cl₂}

{Cu(bis(benzoylpyridine)ethylenediimine)Cl₂}H₂O

Ni(bis(benzoylpyridine)ethylenediimine)Cl₂

Hg₂(N,N'-(bis(pyridin-2-yl)benzylidene)-1,2-ethanediamine)(thiocyanate)4