2,2',3-Trimethoxy-5',6-bis--diphenylether

Base Information

• Chemical Name: 2,2',3-Trimethoxy-5',6-bis--diphenylether
• CAS No.: 87179-88-2
• Molecular Formula: C₂₅H₃₈N₂O₈
• Molecular Weight: 494.585
• Mol file: 87179-88-2.mol

Synonyms:

Chemical Property of 2,2',3-Trimethoxy-5',6-bis--diphenylether

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,2',3-Trimethoxy-5',6-bis--diphenylether

There total 1 articles about 2,2',3-Trimethoxy-5',6-bis--diphenylether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5',6-Diformyl-2,2',3-trimethoxydiphenylether (86750-50-7) + 2,2-dimethoxyethylamine (22483-09-6) → 2,2',3-Trimethoxy-5',6-bis--diphenylether (87179-88-2)

Guidance literature:

With hydrogen; platinum(IV) oxide; Yield given. Multistep reaction; 1.) ethanol, reflux, 1 h;

DOI:10.1002/ardp.19833160809

Reference yield: 89.0%

p-toluenesulfonyl chloride (98-59-9) + 2,2',3-Trimethoxy-5',6-bis--diphenylether (87179-88-2) → 2,2',3-Trimethoxy-5',6-bis--diphenylether

Guidance literature:

With pyridine; for 48h;

DOI:10.1002/ardp.19833160809

Reference yield:

2,2',3-Trimethoxy-5',6-bis--diphenylether (87179-88-2) → 6,6',7-Trimethoxy-7',8-diisoiquinolyl ether (87179-86-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 89 percent / pyridine / 48 h

2: 17 percent / 6 N aq. HCl / dioxane / 4 h / Heating

With pyridine; hydrogenchloride; In 1,4-dioxane;

DOI:10.1002/ardp.19833160809

upstream raw materials:

5',6-Diformyl-2,2',3-trimethoxydiphenylether

2,2-dimethoxyethylamine

Downstream raw materials:

6,6',7-Trimethoxy-7',8-diisoiquinolyl ether