methyl 2-amino-5-bromo-3-methoxybenzoate

Base Information Edit

Chemical Name:methyl 2-amino-5-bromo-3-methoxybenzoate
CAS No.:115378-21-7
Molecular Formula:C9H10BrNO3
Molecular Weight:260.087
Hs Code.:
Mol file:115378-21-7.mol

Synonyms:Benzoic acid,2-amino-5-bromo-3-methoxy-,methyl ester;

Suppliers and Price of methyl 2-amino-5-bromo-3-methoxybenzoate

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
Methyl2-amino-5-bromo-3-methoxybenzoate 97%
1g
$ 589.00

Chemcia Scientific
2-Amino-5-bromo-3-methoxy-benzoicacidmethylester 95%
10 G
$ 1195.00

Total 6 raw suppliers

Chemical Property of methyl 2-amino-5-bromo-3-methoxybenzoate Edit

Chemical Property:

Melting Point:54.5-55 °C
Boiling Point:314.4±37.0 °C(Predicted)
PKA:1.70±0.10(Predicted)
PSA：61.55000
Density:1.531±0.06 g/cm3(Predicted)
LogP:2.40770

Purity/Quality:

98%, ^*data from raw suppliers

Methyl2-amino-5-bromo-3-methoxybenzoate 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of methyl 2-amino-5-bromo-3-methoxybenzoate

There total 9 articles about methyl 2-amino-5-bromo-3-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 5121-34-6
methyl 2-amino-3-methoxybenzoate

: 115378-21-7
methyl 2-amino-5-bromo-3-methoxy-benzoate

Guidance literature:: With N-Bromosuccinimide; In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1039/c39870001528

Reference yield:

: 5307-17-5
methyl 3-methoxy-2-nitrobenzoate

: 115378-21-7
methyl 2-amino-5-bromo-3-methoxy-benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 20 °C / 3102.97 Torr

2: bromine / acetic acid / 1 h / 0 - 20 °C

With palladium 10% on activated carbon; hydrogen; bromine; In methanol; acetic acid;

Reference yield:

: 4920-80-3
3-methoxy-2-nitrobenzoic acid

: 115378-21-7
methyl 2-amino-5-bromo-3-methoxy-benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C

2: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; methanol / 18 h / 20 °C

3: N-Bromosuccinimide / N,N-dimethyl-formamide / 0.5 h / 0 °C

With N-Bromosuccinimide; palladium 10% on activated carbon; hydrogen; potassium carbonate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;