Phosphine, dicyclohexyl(2-methoxyethyl)-

Base Information

Chemical Name:Phosphine, dicyclohexyl(2-methoxyethyl)-
CAS No.:115505-11-8
Molecular Formula:C15H29OP
Molecular Weight:256.368
Hs Code.:
DSSTox Substance ID:DTXSID60423130
Nikkaji Number:J1.611.433B
Wikidata:Q82235256
Mol file:115505-11-8.mol

Synonyms:Phosphine, dicyclohexyl(2-methoxyethyl)-;115505-11-8;SCHEMBL7081792;DTXSID60423130;(2-Methoxyethyl)dicyclohexylphosphine

Suppliers and Price of Phosphine, dicyclohexyl(2-methoxyethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phosphine, dicyclohexyl(2-methoxyethyl)-

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:5
Exact Mass:256.195602542
Heavy Atom Count:17
Complexity:177

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COCCP(C1CCCCC1)C2CCCCC2

Technology Process of Phosphine, dicyclohexyl(2-methoxyethyl)-

There total 1 articles about Phosphine, dicyclohexyl(2-methoxyethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 627-42-9
2-chloroethyl methyl ether

: 829-84-5
dicyclohexylphosphane

: 115505-11-8
dicyclohexyl(2-methoxyethyl)phosphine

Guidance literature:: dicyclohexylphosphane; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In diethyl ether; hexane; at 0 - 20 ℃; for 0.5h; Schlenk technique; Inert atmosphere;

2-chloroethyl methyl ether; In diethyl ether; hexane; at 0 - 20 ℃; for 3h; Schlenk technique; Inert atmosphere;
DOI:10.1021/jacs.8b00928

Reference yield: 95.0%

: (1,5-cyclooctadiene)(3-methylnorborn-2-yl)palladium(II) chloride

: 115505-11-8
dicyclohexyl(2-methoxyethyl)phosphine

: [Cy₂(2-methoxyethyl)P]Pd(3-CH₃norborn-2-yl)Cl

Guidance literature:: In dichloromethane; at 20 ℃; for 0.166667h; Glovebox; Inert atmosphere;
DOI:10.1021/jacs.8b00928

Reference yield: 92.0%

: 14878-21-8,18953-16-7
cis-{Os(CO)4Br₂}

: 115505-11-8
dicyclohexyl(2-methoxyethyl)phosphine

: 138151-15-2
cis-dibromo-cis-dicarbonyl-trans-bis{dicyclohexyl(2-methoxyethyl)phosphane-P}osmium

Guidance literature:: In tetrahydrofuran; Ar atmosphere; refluxing (1.5 h); partial evapn. (vac.), pptn. on addn. of hexane, washing (hexane), filtration, drying (vac.), boiling in EtOH, crystn. (-30°C), sepn., drying (vac.); elem. anal.;