Dithiophosphoric acid O-benzotriazol-1-yl ester O'-[(2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl] ester S-methyl ester

Base Information

• Chemical Name: Dithiophosphoric acid O-benzotriazol-1-yl ester O'-[(2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl] ester S-methyl ester
• CAS No.: 130674-92-9
• Molecular Formula: C₃₈H₃₈N₅O₈PS₂
• Molecular Weight: 787.854

Synonyms:

Chemical Property of Dithiophosphoric acid O-benzotriazol-1-yl ester O'-[(2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl] ester S-methyl ester

Chemical Property:

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Useful:

Technology Process of Dithiophosphoric acid O-benzotriazol-1-yl ester O'-[(2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl] ester S-methyl ester

There total 2 articles about Dithiophosphoric acid O-benzotriazol-1-yl ester O'-[(2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl] ester S-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzotriazol-1-ol (2592-95-2) → Dithiophosphoric acid O-benzotriazol-1-yl ester O'-[(2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl] ester S-methyl ester (130674-92-9)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / dioxane / 1 h

2: acetonitrile

With pyridine; In 1,4-dioxane; acetonitrile;

DOI:10.1016/S0040-4039(00)97430-6

Reference yield:

Dithiophosphoric acid O,O'-dibenzotriazol-1-yl ester S-methyl ester (130659-70-0) + 5'-O-(4-4'-dimethoxytrityl)thymidine (40615-39-2) → Dithiophosphoric acid O-benzotriazol-1-yl ester O'-[(2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl] ester S-methyl ester (130674-92-9)

Guidance literature:

In acetonitrile;

DOI:10.1016/S0040-4039(00)97430-6

Reference yield:

Dithiophosphoric acid O-benzotriazol-1-yl ester O'-[(2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl] ester S-methyl ester (130674-92-9) → C32H34N2O8PS2(1-)

Guidance literature:

With pyridine; water;

DOI:10.1016/S0040-4039(00)97430-6

upstream raw materials:

Dithiophosphoric acid O,O'-dibenzotriazol-1-yl ester S-methyl ester

5'-O-(4-4'-dimethoxytrityl)thymidine

benzotriazol-1-ol

Downstream raw materials:

C₄₄H₄₉N₄O₁₃PS₂

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