3-methyl-1,5-diphenyl-2-chloropentane-1,5-dione phenylhydrazone

Base Information

Chemical Name:3-methyl-1,5-diphenyl-2-chloropentane-1,5-dione phenylhydrazone
CAS No.:943987-94-8
Molecular Formula:C₂₄H₂₃ClN₂O
Molecular Weight:390.912
Hs Code.:

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Chemical Property of 3-methyl-1,5-diphenyl-2-chloropentane-1,5-dione phenylhydrazone

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Technology Process of 3-methyl-1,5-diphenyl-2-chloropentane-1,5-dione phenylhydrazone

There total 2 articles about 3-methyl-1,5-diphenyl-2-chloropentane-1,5-dione phenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 122603-44-5
3-methyl-1,5-diphenyl-2-chloro-1,5-pentanedione

: 100-63-0
phenylhydrazine

: 943987-94-8
3-methyl-1,5-diphenyl-2-chloropentane-1,5-dione phenylhydrazone

Guidance literature:: In ethanol; acetic acid; for 1h;
DOI:10.1134/S1070428007020108

Reference yield:

: 1226-91-1
3-methyl-1,5-diphenyl-pentane-1,5-dione

: 943987-94-8
3-methyl-1,5-diphenyl-2-chloropentane-1,5-dione phenylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: BTMAICl₂ / acetic acid

2: 66 percent / acetic acid; ethanol / 1 h

With N,N,N-trimethylbenzenemethanaminium dichloroiodate; In ethanol; acetic acid;
DOI:10.1134/S1070428007020108