3-((E)-3-Phenyl-allyl)-pentanedioic acid diethyl ester

Base Information

Chemical Name:3-((E)-3-Phenyl-allyl)-pentanedioic acid diethyl ester
CAS No.:117213-96-4
Molecular Formula:C₁₈H₂₄O₄
Molecular Weight:304.386
Hs Code.:

Synonyms:

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Chemical Property of 3-((E)-3-Phenyl-allyl)-pentanedioic acid diethyl ester

Chemical Property:

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Technology Process of 3-((E)-3-Phenyl-allyl)-pentanedioic acid diethyl ester

There total 1 articles about 3-((E)-3-Phenyl-allyl)-pentanedioic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 796104-41-1
ethyl (2E,5E)-6-phenyl-2,5-hexadienoate

: 105-53-3
diethyl malonate

: 117213-96-4
3-((E)-3-Phenyl-allyl)-pentanedioic acid diethyl ester

Guidance literature:: With 1.) base; Multistep reaction;
DOI:10.1016/S0040-4039(00)80391-3

Reference yield:

: 117213-96-4
3-((E)-3-Phenyl-allyl)-pentanedioic acid diethyl ester

: 146501-49-7
(R)-4-((E)-3-Phenyl-allyl)-tetrahydro-pyran-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: H₂O / acetone / PLE, pH 8.0

2: LiBH₄

3: Ac₂O, Py

With pyridine; lithium borohydride; water; acetic anhydride; In acetone;

Reference yield:

: 117213-96-4
3-((E)-3-Phenyl-allyl)-pentanedioic acid diethyl ester

: (R)-2-{(2R,4R)-4-[(E)-4-(tert-Butyl-diphenyl-silanyloxy)-but-2-enyl]-6-methoxy-tetrahydro-pyran-2-yl}-propan-1-ol

Guidance literature:: Multi-step reaction with 23 steps

1: H₂O / acetone / PLE, pH 8.0

2: LiBH₄

3: Ac₂O, Py

6: LiAlH₄

7: NaH

8: 1.) O₃, 2.) Me₂S

9: Et₃N

10: 51 percent / KN(SiMe₃)2, 18-crown-6

11: DIBAL

12: Py

13: 1.) thexylborane, 2.) NaOH, H₂O₂

14: Ag₂CO₃, celite

15: DIBAL

16: BF₃*OEt₂

17: H⁺

18: H₂ / Pd(OH)2

19: Swern oxidation

20: t-BuOK

21: DIBAL

22: imidazole

23: PPTS

With pyridine; 1H-imidazole; sodium hydroxide; lithium aluminium tetrahydride; lithium borohydride; 18-crown-6 ether; dimethylsulfide; Celite; thexylborane; boron trifluoride diethyl etherate; potassium tert-butylate; water; hydrogen; dihydrogen peroxide; pyridinium p-toluenesulfonate; acetic anhydride; hydrogen cation; potassium hexamethylsilazane; sodium hydride; diisobutylaluminium hydride; ozone; triethylamine; silver carbonate; palladium dihydroxide; In acetone;