(CH₃CH₂CH₂CH₂)3SnCH(C₆H₅)CH₂COCH₃

Base Information

Chemical Name:(CH₃CH₂CH₂CH₂)3SnCH(C₆H₅)CH₂COCH₃
CAS No.:36163-91-4
Molecular Formula:C₂₂H₃₈OSn
Molecular Weight:437.253
Hs Code.:

(CH<sub>3</sub>CH<sub>2</sub>CH<sub>2</sub>CH<sub>2</sub>)3SnCH(C<sub>6</sub>H<sub>5</sub>)CH<sub>2</sub>COCH<sub>3</sub>

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Chemical Property of (CH₃CH₂CH₂CH₂)3SnCH(C₆H₅)CH₂COCH₃

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Technology Process of (CH₃CH₂CH₂CH₂)3SnCH(C₆H₅)CH₂COCH₃

There total 2 articles about (CH₃CH₂CH₂CH₂)3SnCH(C₆H₅)CH₂COCH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 27262-82-4
tributylstannylmagnesium chloride

: 122-57-6
1-Phenylbut-1-en-3-one

: 36163-91-4
(CH₃CH₂CH₂CH₂)3SnCH(C₆H₅)CH₂COCH₃

Guidance literature:: DOI:10.1016/S0022-328X(00)80788-3

Reference yield: 18.0%

: 4226-01-1
tri-n-butyltin lithium

: 122-57-6
1-Phenylbut-1-en-3-one

: 36163-91-4
(CH₃CH₂CH₂CH₂)3SnCH(C₆H₅)CH₂COCH₃

Guidance literature:: With water; In tetrahydrofuran; enone in anhyd. THF added dropwise over 5 min to stirred soln. of Bu3SnLi in anhyd. THF under N2 at -100 °C, stirred for 5 min, added H2O; extd. with Et2O, dried (MgSO4), evapd. in vac., flash chromd. (Kieselgel 60, Et2O/light petroleum 5/95);
DOI:10.1016/0022-328X(85)87366-6

Reference yield: 43.0%

: 36163-91-4
(CH₃CH₂CH₂CH₂)3SnCH(C₆H₅)CH₂COCH₃

: (2RS,4SR)-2,4-diphenyl-4-tributyltinbutan-2-ol

: (2RS,4RS)-2,4-diphenyl-4-tributyltinbutan-2-ol

Guidance literature:: With water; phenylmagnesium bromide; In diethyl ether; soln. of PhMgBr in Et2O added dropwise to stirred soln. of ketone in anhyd. Et2O under N2 at 0 °C, stirred for 1 h, added cautiously H2O; extd. (Et2O), org. layer dried (MgSO4), evapd. in vac., flash chromd. (Kieselgel 60, Et2O/light petroleum);
DOI:10.1016/0022-328X(85)87366-6