C₂₄H₃₄N₂O₄SSi

Base Information

• Chemical Name: C₂₄H₃₄N₂O₄SSi
• CAS No.: 1310373-13-7
• Molecular Formula: C₂₄H₃₄N₂O₄SSi
• Molecular Weight: 474.696
• Mol file: 1310373-13-7.mol

Synonyms:

Chemical Property of C₂₄H₃₄N₂O₄SSi

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₃₄N₂O₄SSi

There total 2 articles about C₂₄H₃₄N₂O₄SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

C17H26O3Si (1310352-91-0) + toluene-4-sulfonic acid hydrazide (1576-35-8) → C24H34N2O4SSi (1310373-13-7)

Guidance literature:

In methanol; for 5h; Reflux;

DOI:10.1080/15421401003604203

Reference yield:

3-trimethylsilyl-1-propanol (2917-47-7) + 5-oxo-5-phenylvaleric acid (1501-05-9) → C24H34N2O4SSi (1310373-13-7)

Guidance literature:

Multi-step reaction with 2 steps

1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere

2: methanol / 5 h / Reflux

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; 1: Fischer esterification;

DOI:10.1080/15421401003604203

upstream raw materials:

C₁₇H₂₆O₃Si

toluene-4-sulfonic acid hydrazide

3-trimethylsilyl-1-propanol

5-oxo-5-phenylvaleric acid

Refernces