3-carbamoyl-1-[2-(2-methyl-5-nitro-1H-imidazol-1-yl)ethyl]pyridinium chloride

Base Information

Chemical Name:3-carbamoyl-1-[2-(2-methyl-5-nitro-1H-imidazol-1-yl)ethyl]pyridinium chloride
CAS No.:96515-31-0
Molecular Formula:C₁₂H₁₄N₅O₃*Cl
Molecular Weight:311.728
Hs Code.:

Synonyms:Pyridinium,3-(aminocarbonyl)-1-[2-(2-methyl-5-nitro-1H-imidazol-1-yl)ethyl]-, chloride(9CI); 1-[2-(2-Methyl-5-nitro-1-imidazolyl)ethyl]-3-carbamoylpyridiniumchloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-carbamoyl-1-[2-(2-methyl-5-nitro-1H-imidazol-1-yl)ethyl]pyridinium chloride

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Technology Process of 3-carbamoyl-1-[2-(2-methyl-5-nitro-1H-imidazol-1-yl)ethyl]pyridinium chloride

There total 2 articles about 3-carbamoyl-1-[2-(2-methyl-5-nitro-1H-imidazol-1-yl)ethyl]pyridinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 98-92-0,1255150-40-3
nicotinamide

: 13182-81-5
1-(2-chloroethyl)-2-methyl-5-nitro-1H-imidazole

: 96515-31-0
Chlorure de <(methyl-2 nitro-5 imidazol-1-yl)-2 ethyl>-1 carbamoyl-3 pyridinium

Guidance literature:: In N,N-dimethyl-formamide; at 128 ℃; for 96h;
DOI:10.1002/jhet.5570210615

Reference yield:

: 443-48-1
metronidazole

: 96515-31-0
Chlorure de <(methyl-2 nitro-5 imidazol-1-yl)-2 ethyl>-1 carbamoyl-3 pyridinium

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / SOCl₂ / 3 h / Heating

2: 86 percent / dimethylformamide / 96 h / 128 °C

With thionyl chloride; In N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570210615