C₂₇H₄₃BrN₂O₇Si

Base Information

Chemical Name:C₂₇H₄₃BrN₂O₇Si
CAS No.:1357622-60-6
Molecular Formula:C₂₇H₄₃BrN₂O₇Si
Molecular Weight:615.637
Hs Code.:

C<sub>27</sub>H<sub>43</sub>BrN<sub>2</sub>O<sub>7</sub>Si

Synonyms:

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Chemical Property of C₂₇H₄₃BrN₂O₇Si

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Technology Process of C₂₇H₄₃BrN₂O₇Si

There total 24 articles about C₂₇H₄₃BrN₂O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1357622-39-9
(S)-1-(tert-butyl)dimethylsilyloxy-2-((3-bromophenoxy)methyl)-3-isocyanopropane

: 625-45-6
2-methoxyacetic acid

: (3aS,6aR)-2,2-Dimethyl-4,6a-dihydro-3aH-[1,3]dioxolo[4,5-c]pyrrole

: 1357622-60-6
C₂₇H₄₃BrN₂O₇Si

Guidance literature:: In methanol; at 20 ℃; for 48h; diastereoselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1039/c1ob06632c

Reference yield:

: 1357622-26-4
(R,E)-2-(3-bromophenoxy)methyl-5-methylhex-3-enyl acetate

: 1357622-60-6
C₂₇H₄₃BrN₂O₇Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: potassium hydroxide / methanol / 0 °C

2.1: triethylamine / dichloromethane / -30 °C / Inert atmosphere

3.1: sodium azide / N,N-dimethyl-formamide / 50 °C / Inert atmosphere

4.1: triphenylphosphine / tetrahydrofuran; water / 0 - 50 °C / Inert atmosphere

5.1: dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C / Inert atmosphere

6.1: ozone / methanol; dichloromethane / -78 °C / Inert atmosphere

6.2: -78 °C / Inert atmosphere

7.1: sodium tetrahydroborate / methanol; dichloromethane / -78 - -3 °C / Inert atmosphere

8.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

9.1: triethylamine; trichlorophosphate / dichloromethane / -30 °C / Inert atmosphere

10.1: methanol / 48 h / 20 °C / Inert atmosphere; Molecular sieve

With 1H-imidazole; sodium tetrahydroborate; sodium azide; ozone; triethylamine; dicyclohexyl-carbodiimide; triphenylphosphine; potassium hydroxide; trichlorophosphate; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; 10.1: Ugi condensation;
DOI:10.1039/c1ob06632c

Reference yield:

: 591-20-8
3-Bromophenol

: 1357622-60-6
C₂₇H₄₃BrN₂O₇Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: di-tert-butyl-diazodicarboxylate; triphenylphosphine / dichloromethane / 2.1 h / 0 - 20 °C / Inert atmosphere

2.1: potassium hydroxide / methanol / 0 °C

3.1: triethylamine / dichloromethane / -30 °C / Inert atmosphere

4.1: sodium azide / N,N-dimethyl-formamide / 50 °C / Inert atmosphere

5.1: triphenylphosphine / tetrahydrofuran; water / 0 - 50 °C / Inert atmosphere

6.1: dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C / Inert atmosphere

7.1: ozone / methanol; dichloromethane / -78 °C / Inert atmosphere

7.2: -78 °C / Inert atmosphere

8.1: sodium tetrahydroborate / methanol; dichloromethane / -78 - -3 °C / Inert atmosphere

9.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

10.1: triethylamine; trichlorophosphate / dichloromethane / -30 °C / Inert atmosphere

11.1: methanol / 48 h / 20 °C / Inert atmosphere; Molecular sieve

With 1H-imidazole; sodium tetrahydroborate; sodium azide; di-tert-butyl-diazodicarboxylate; ozone; triethylamine; dicyclohexyl-carbodiimide; triphenylphosphine; potassium hydroxide; trichlorophosphate; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; 11.1: Ugi condensation;
DOI:10.1039/c1ob06632c