Zr(η5-C5H5)2(OC(CH3)2CH2P(C(CH3)3)2))(B(C6F5)3(CH3))

Base Information

Chemical Name:Zr(η5-C5H5)2(OC(CH3)2CH2P(C(CH3)3)2))(B(C6F5)3(CH3))
CAS No.:1370365-53-9
Molecular Formula:C₁₉H₃BF₁₅*C₂₂H₃₆OPZr
Molecular Weight:965.745
Hs Code.:

Synonyms:

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Chemical Property of Zr(η5-C5H5)2(OC(CH3)2CH2P(C(CH3)3)2))(B(C6F5)3(CH3))

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Technology Process of Zr(η5-C5H5)2(OC(CH3)2CH2P(C(CH3)3)2))(B(C6F5)3(CH3))

There total 2 articles about Zr(η5-C5H5)2(OC(CH3)2CH2P(C(CH3)3)2))(B(C6F5)3(CH3)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1309604-77-0
2,6-di-tert-butylpyridininum tetrakis(pentafluorophenyl)borate

: 1370365-46-0
Zr(η5-C5H5)2(P(C(CH3)3)2CH2C(CH3)2O)(CH3)

: 1370365-53-9
Zr(η5-C5H5)2(OC(CH3)2CH2P(C(CH3)3)2))(B(C6F5)3(CH3))

Guidance literature:: In fluorobenzene; Ar, Schlenk-line and glovebox; soln. of pyridinium salt added dropwise to soln. of Zr-complex; not isolated; detd. by (31)P NMR and MAS;
DOI:10.1002/ejic.201100968

Reference yield:

: 1370365-46-0
Zr(η5-C5H5)2(P(C(CH3)3)2CH2C(CH3)2O)(CH3)

: 1109-15-5
tris(pentafluorophenyl)borate

: 1370365-53-9
Zr(η5-C5H5)2(OC(CH3)2CH2P(C(CH3)3)2))(B(C6F5)3(CH3))

Guidance literature:: In hexane; Ar, Schlenk-line and glovebox; soln. of B(C6F5)3 and soln. of Zr-complexmixed in Schlenk flask; supernatant decanted, oil washed (hexane), dried (vac.); not isolated, detd. by NMR;
DOI:10.1002/ejic.201100968

Reference yield:

: 1370365-53-9
Zr(η5-C5H5)2(OC(CH3)2CH2P(C(CH3)3)2))(B(C6F5)3(CH3))

: 1333-74-0
hydrogen

: Zr(η5-C5H5)2(OC(CH3)2CH2P(C(CH3)3)2))(B(C6F5)3H)

Guidance literature:: In fluorobenzene; ⁽²⁾H₈-toluene; Ar, Schlenk-line and glovebox; soln. of Zr-complex prepared in NMR tube fitted with Teflon needle valve, tube removed, connected to Schlenk line, subjected to three freeze-pump-thaw degassing cycles, back-filled with1 bar H2 at room temp.; after several d oil septd.; detd. by NMR;
DOI:10.1002/ejic.201100968