p-(methanesulfonyl)phenyl chlorotetrafluoride

Base Information

Chemical Name:p-(methanesulfonyl)phenyl chlorotetrafluoride
CAS No.:1393937-26-2
Molecular Formula:C₇H₇ClF₄O₂S₂
Molecular Weight:298.71
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-(methanesulfonyl)phenyl chlorotetrafluoride

Chemical Property:

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Technology Process of p-(methanesulfonyl)phenyl chlorotetrafluoride

There total 4 articles about p-(methanesulfonyl)phenyl chlorotetrafluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 92424-06-1
bis[4-(methanesulfonyl)phenyl] disulfide

: 1393937-26-2
p-(methanesulfonyl)phenyl chlorotetrafluoride

Guidance literature:: With potassium fluoride; chlorine; In acetonitrile; at 20 ℃; Cooling with ice; Inert atmosphere;
DOI:10.3762/bjoc.8.53

Reference yield:

: 1393937-27-3
4-(tert-butylthio)phenyl methyl sulfone

: 1393937-26-2
p-(methanesulfonyl)phenyl chlorotetrafluoride

Guidance literature:: Multi-step reaction with 3 steps

1: aluminum (III) chloride / toluene / 4 h / 20 °C / Inert atmosphere

2: bromine; acetic acid / n-heptane; dichloromethane / 3 h

3: potassium fluoride; chlorine / acetonitrile / 20 °C / Cooling with ice; Inert atmosphere

With aluminum (III) chloride; potassium fluoride; bromine; chlorine; acetic acid; In n-heptane; dichloromethane; toluene; acetonitrile;
DOI:10.3762/bjoc.8.53

Reference yield:

: 3814-25-3
4-(methylsulfonyl)benzenethiol

: 1393937-26-2
p-(methanesulfonyl)phenyl chlorotetrafluoride

Guidance literature:: Multi-step reaction with 2 steps

1: bromine; acetic acid / n-heptane; dichloromethane / 3 h

2: potassium fluoride; chlorine / acetonitrile / 20 °C / Cooling with ice; Inert atmosphere

With potassium fluoride; bromine; chlorine; acetic acid; In n-heptane; dichloromethane; acetonitrile;
DOI:10.3762/bjoc.8.53