(benzylideneisocyanamide)pentacarbonyltungsten

Base Information

Chemical Name:(benzylideneisocyanamide)pentacarbonyltungsten
CAS No.:73789-70-5
Molecular Formula:C₁₃H₆N₂O₅W
Molecular Weight:454.051
Hs Code.:

Synonyms:

Suppliers and Price of (benzylideneisocyanamide)pentacarbonyltungsten

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (benzylideneisocyanamide)pentacarbonyltungsten

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (benzylideneisocyanamide)pentacarbonyltungsten

There total 1 articles about (benzylideneisocyanamide)pentacarbonyltungsten which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 73804-82-7
pentacarbonyl[(N-isocyanimino)triphenylphosphorane]tungsten

: 100-52-7
benzaldehyde

: 73789-70-5
(benzylideneisocyanamide)pentacarbonyltungsten

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; byproducts: OP(C6H5)3; all manipulations under N2; addn. of the carbonyl compound to a THF soln. of the complex; introduction of a stream of dry HCl gas into the soln. (4 s); color changed to deep red for a short time; 24 h, 40°C;; evapn. under high vac.; dissolving in CH2Cl2; chromy. (silica/n-hexane,CH2Cl2/n-hexane 3:1, collecting the first band); crystn. (n-hexane, 0°C); elem. anal.;;

Reference yield: 60.0%

: 73789-70-5
(benzylideneisocyanamide)pentacarbonyltungsten

: 95527-90-5
pentacarbonyl[(benzylidenehydrazino)(methylamino)carbene]tungsten

Guidance literature:: With methylamine; In tetrahydrofuran; Petroleum ether; all manipulations under N2; addn. of a THF soln. of methylamine to the complex in petroleum ether at room temp.; reaction for 2-3 h;; removal of volatiles; drying under high vac.; dissolving in EtOH; pptn.by addn. of H2O; drying under high vac.; elem. anal.;;