tetrachloro{1,4-bis(p-methoxyphenyl)-2,3-dimethyl-1,4-diazabutadiene}tin(IV)

Base Information

Chemical Name:tetrachloro{1,4-bis(p-methoxyphenyl)-2,3-dimethyl-1,4-diazabutadiene}tin(IV)
CAS No.:125429-70-1
Molecular Formula:C₁₈H₂₀Cl₄N₂O₂Sn
Molecular Weight:556.891
Hs Code.:

Synonyms:

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Chemical Property of tetrachloro{1,4-bis(p-methoxyphenyl)-2,3-dimethyl-1,4-diazabutadiene}tin(IV)

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Technology Process of tetrachloro{1,4-bis(p-methoxyphenyl)-2,3-dimethyl-1,4-diazabutadiene}tin(IV)

There total 2 articles about tetrachloro{1,4-bis(p-methoxyphenyl)-2,3-dimethyl-1,4-diazabutadiene}tin(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 19215-52-2
1,4-bis(p-methoxyphenyl)-2,3-dimethyl-1,4-diazabutadiene

: 7646-78-8
tin(IV) chloride

: 125429-70-1
tetrachloro{1,4-bis(p-methoxyphenyl)-2,3-dimethyl-1,4-diazabutadiene}tin(IV)

Guidance literature:: In tetrachloromethane; under N2; addn. of SnCl4 (distd. under N2) in CCl4 to a soln. of (CH3OC6H4)2(N(C2H3))2 in CCl4 with stirring; stirred for 30 min.;; filtered, washed after first pptn. continously with CCl4; elem. anal.;;

Reference yield:

: 1,4-di(p-methoxyphenyl)-2,3-dimethyl-1,4-diazabutadiene

: 7646-78-8
tin(IV) chloride

: 125429-70-1
tetrachloro{1,4-di(p-methoxyphenyl)-2,3-dimethyl-1,4-diazabutadiene}tin(IV)

Guidance literature:: In tetrachloromethane; preparation in a vacuum line or in dry-box filled with dry nitrogen; stirring for about 30 min after 1st ppt. is observed; chem. anal.;
DOI:10.1007/BF00811122