C₂₂H₂₂N₂O₃S

Base Information

Chemical Name:C₂₂H₂₂N₂O₃S
CAS No.:78012-22-3
Molecular Formula:C₂₂H₂₂N₂O₃S
Molecular Weight:394.494
Hs Code.:

C<sub>22</sub>H<sub>22</sub>N<sub>2</sub>O<sub>3</sub>S

Synonyms:

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Chemical Property of C₂₂H₂₂N₂O₃S

Chemical Property:

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Technology Process of C₂₂H₂₂N₂O₃S

There total 9 articles about C₂₂H₂₂N₂O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78012-21-2
5,10-dihydro-6,7-dimethyl-4H-benzo<5,6>cyclohepta<1,2-b>furan-10-one

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 78012-22-3
C₂₂H₂₂N₂O₃S

Guidance literature:: With toluene-4-sulfonic acid; In ethanol; at 80 ℃; for 16h;
DOI:10.1039/P19810003087

Reference yield:

: 5724-56-1
2,3-dimethylbenzonitrile

: 78012-22-3
C₂₂H₂₂N₂O₃S

Guidance literature:: Multi-step reaction with 9 steps

1: 96 percent / aq. potassium hydroxide

2: 62 percent / lithium aluminium hydride / tetrahydrofuran

3: 98 percent / pyridinium chlorochromate / CH₂Cl₂

4: 45 percent / sodium hydride, 15-crown-5 / bis-(2-methoxy-ethyl) ether / 1) 80 deg C, 1.5 h; 2) room temperature, 1 h

5: 54 percent / hydrogen, chlorotris(triphenylphosphine)rhodium / ethanol; benzene / 336 h / 70 °C / 121600 Torr

6: 69 percent / aq. sodium hydroxide / ethanol / 1 h / Heating

7: thionyl chloride / benzene / 2 h / Heating

8: 7.52 g / aluminium chloride / nitrobenzene / 1) room temperature, 16 h; 2) 80 deg C, 4 h

9: toluene-4-sulphonic acid / ethanol / 16 h / 80 °C

With potassium hydroxide; sodium hydroxide; Wilkinson's catalyst; lithium aluminium tetrahydride; aluminium trichloride; thionyl chloride; 15-crown-5; hydrogen; sodium hydride; toluene-4-sulfonic acid; pyridinium chlorochromate; In tetrahydrofuran; ethanol; dichloromethane; diethylene glycol dimethyl ether; nitrobenzene; benzene;
DOI:10.1039/P19810003087

Reference yield:

: 5779-93-1
2,3-dimethylbenzaldehyde

: 78012-22-3
C₂₂H₂₂N₂O₃S

Guidance literature:: Multi-step reaction with 6 steps

1: 45 percent / sodium hydride, 15-crown-5 / bis-(2-methoxy-ethyl) ether / 1) 80 deg C, 1.5 h; 2) room temperature, 1 h

2: 54 percent / hydrogen, chlorotris(triphenylphosphine)rhodium / ethanol; benzene / 336 h / 70 °C / 121600 Torr

3: 69 percent / aq. sodium hydroxide / ethanol / 1 h / Heating

4: thionyl chloride / benzene / 2 h / Heating

5: 7.52 g / aluminium chloride / nitrobenzene / 1) room temperature, 16 h; 2) 80 deg C, 4 h

6: toluene-4-sulphonic acid / ethanol / 16 h / 80 °C

With sodium hydroxide; Wilkinson's catalyst; aluminium trichloride; thionyl chloride; 15-crown-5; hydrogen; sodium hydride; toluene-4-sulfonic acid; In ethanol; diethylene glycol dimethyl ether; nitrobenzene; benzene;
DOI:10.1039/P19810003087