Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2⁽¹⁺⁾*C₅H₅^(1-)*C₄H₈O=(Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2)C₅H₅*C₄H₈O

Base Information

• Chemical Name: Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2⁽¹⁺⁾*C₅H₅^(1-)*C₄H₈O=(Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2)C₅H₅*C₄H₈O
• CAS No.: 100228-74-8
• Molecular Formula: C₄H₈O*C₅H₅*C₅₂H₄₈IrP₄
• Molecular Weight: 1126.27

Synonyms:

Chemical Property of Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2⁽¹⁺⁾*C₅H₅^(1-)*C₄H₈O=(Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2)C₅H₅*C₄H₈O

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Technology Process of Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2⁽¹⁺⁾*C₅H₅^(1-)*C₄H₈O=(Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2)C₅H₅*C₄H₈O

There total 1 articles about Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2⁽¹⁺⁾*C₅H₅^(1-)*C₄H₈O=(Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2)C₅H₅*C₄H₈O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

Ir((C6H5)2PCH2CH2P(C6H5)2)2(1+)*Cl(1-)=Ir((C6H5)2PCH2CH2P(C6H5)2)2Cl (15390-38-2) + cyclopentadienyllithium (16733-97-4) → Ir((C6H5)2PCH2CH2P(C6H5)2)2(1+)*C5H5(1-)*C4H8O=(Ir((C6H5)2PCH2CH2P(C6H5)2)2)C5H5*C4H8O (100228-74-8)

Guidance literature:

In tetrahydrofuran; a freshly prepd. THF soln. of CpLi was added under N2 to a suspn. of Ir-complex in THF until all the complex dissolved; Et2O was slowly added, ppt. collected; elem. anal.;

DOI:10.1021/om00135a025

Reference yield:

tetrafluoroboric acid diethyl ether (67969-82-8) + Ir((C6H5)2PCH2CH2P(C6H5)2)2(1+)*C5H5(1-)*C4H8O=(Ir((C6H5)2PCH2CH2P(C6H5)2)2)C5H5*C4H8O (100228-74-8) → IrHCl((C6H5)2PCH2CH2P(C6H5)2)2(1+)*BF4(1-)=(IrHCl((C6H5)2PCH2CH2P(C6H5)2)2)BF4 (79292-53-8)

Guidance literature:

In dichloromethane; HBF4*OEt2 was added to a soln. of Ir-complex under H2 atmosphere until the colour of the soln. changed from red to light yellow; n-hexane was added, ppt. collected; identified by (1)H NMR and IR spectral data;

DOI:10.1021/om00135a025

upstream raw materials:

Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2⁽¹⁺⁾*Cl^(1-)=Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2Cl

cyclopentadienyllithium

Downstream raw materials:

IrHCl((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2⁽¹⁺⁾*BF₄^(1-)=(IrHCl((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2)BF₄

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