[μ2-(SR)2bis[η-(3-phenyl-3-thiapropyl)cyclopentadienyl]dichloromolybdenum](cycloocta-1,4-diene)rhodium hexafluorophosphate

Base Information

Chemical Name:[μ2-(SR)2bis[η-(3-phenyl-3-thiapropyl)cyclopentadienyl]dichloromolybdenum](cycloocta-1,4-diene)rhodium hexafluorophosphate
CAS No.:98183-65-4
Molecular Formula:C₃₄H₃₈Cl₂MoRhS₂*Cl
Molecular Weight:816.012
Hs Code.:

[μ2-(SR)2bis[η-(3-phenyl-3-thiapropyl)cyclopentadienyl]dichloromolybdenum](cycloocta-1,4-diene)rhodium hexafluorophosphate

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Chemical Property of [μ2-(SR)2bis[η-(3-phenyl-3-thiapropyl)cyclopentadienyl]dichloromolybdenum](cycloocta-1,4-diene)rhodium hexafluorophosphate

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Technology Process of [μ2-(SR)2bis[η-(3-phenyl-3-thiapropyl)cyclopentadienyl]dichloromolybdenum](cycloocta-1,4-diene)rhodium hexafluorophosphate

There total 1 articles about [μ2-(SR)2bis[η-(3-phenyl-3-thiapropyl)cyclopentadienyl]dichloromolybdenum](cycloocta-1,4-diene)rhodium hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 12092-47-6
di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium

: 86857-67-2
Mo(C₅H₄CH₂CH₂SC₆H₅)2Cl₂

: 98183-65-4
[μ2-(SR)2bis[η-(3-phenyl-3-thiapropyl)cyclopentadienyl]dichloromolybdenum](cycloocta-1,4-diene)rhodium hexafluorophosphate

Guidance literature:: In acetone; (inert gas); to suspn. of Mo complex was added soln. of Rh complex and stirred for 4 h at 40°C; cool soln. was evapd. in vac., residue extd. with acetone, concd. soln.was cooled to -78°C, yielding green powder within 24 h, it was washed with Et2O and dried in vac.; elem. anal.;
DOI:10.1016/0022-328X(85)87172-2