2,2,5,5-tetramethyl-3-imidazolin-1-oxyl-4-O-benzoylhydroximic acid chloride hydrochloride

Base Information

Chemical Name:2,2,5,5-tetramethyl-3-imidazolin-1-oxyl-4-O-benzoylhydroximic acid chloride hydrochloride
CAS No.:134279-92-8
Molecular Formula:C₁₅H₁₇ClN₃O₃*ClH
Molecular Weight:359.232
Hs Code.:

Synonyms:

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Chemical Property of 2,2,5,5-tetramethyl-3-imidazolin-1-oxyl-4-O-benzoylhydroximic acid chloride hydrochloride

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Technology Process of 2,2,5,5-tetramethyl-3-imidazolin-1-oxyl-4-O-benzoylhydroximic acid chloride hydrochloride

There total 4 articles about 2,2,5,5-tetramethyl-3-imidazolin-1-oxyl-4-O-benzoylhydroximic acid chloride hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 134279-78-0
C₁₅H₁₇ClN₃O₃

: 134279-92-8
2,2,5,5-tetramethyl-3-imidazolin-1-oxyl-4-O-benzoylhydroximic acid chloride hydrochloride

Guidance literature:: With hydrogenchloride; In diethyl ether; at 20 ℃; for 24h;
DOI:10.1007/BF00965436

Reference yield:

: 60829-54-1
2,2,5,5-tetramethyl-4-nitromethyleneimidazolidine-1-oxyl

: 134279-92-8
2,2,5,5-tetramethyl-3-imidazolin-1-oxyl-4-O-benzoylhydroximic acid chloride hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: benzoyl chloride, NEt₃ / CHCl₃ / 0.25 h / 0 °C

2: 60 percent / HCl / diethyl ether / 24 h / 20 °C / other nucleophiles

With hydrogenchloride; benzoyl chloride; triethylamine; In diethyl ether; chloroform;
DOI:10.1007/BF00965436

Reference yield:

: 98-88-4
benzoyl chloride

: 134279-92-8
2,2,5,5-tetramethyl-3-imidazolin-1-oxyl-4-O-benzoylhydroximic acid chloride hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: NEt₃ / tetrahydrofuran / 0.5 h / 20 °C

2: 60 percent / HCl / diethyl ether / 24 h / 20 °C / other nucleophiles

With hydrogenchloride; triethylamine; In tetrahydrofuran; diethyl ether;
DOI:10.1007/BF00965436