[Ti(2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridine)Cl₃]AlCl₄

Base Information

Chemical Name:[Ti(2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridine)Cl₃]AlCl₄
CAS No.:850196-07-5
Molecular Formula:AlCl₄*C₃₃H₄₃Cl₃N₃Ti
Molecular Weight:804.757
Hs Code.:

[Ti(2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridine)Cl<sub>3</sub>]AlCl<sub>4</sub>

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Chemical Property of [Ti(2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridine)Cl₃]AlCl₄

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Technology Process of [Ti(2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridine)Cl₃]AlCl₄

There total 2 articles about [Ti(2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridine)Cl₃]AlCl₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 7446-70-0
aluminium trichloride

: 850196-08-6,850196-05-3
[Ti(2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridine)Cl₄]

: 850196-07-5
[Ti(2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridine)Cl₃]AlCl₄

Guidance literature:: In dichloromethane; under Ar; soln. of Ti complex in CH2Cl2 added to AlCl3 (molar ratio 1:1.08); stirred at room temp. for 16 h; heated at reflux for 9 h; volatiles removed in vac. at room temp.; toluene added; filtered; ppt. washed with toluene; dried in vac. at room temp.; elem. anal.;
DOI:10.1039/b415997g

Reference yield:

: 850196-08-6,850196-05-3
[Ti(2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridine)Cl₃]Cl

: 850196-07-5
[Ti(2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridine)Cl₃]AlCl₄

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran

2: toluene

3: dichloromethane

In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1039/b415997g