methyl (-E-3-methyl)cinnamate

Base Information

Chemical Name:methyl (-E-3-methyl)cinnamate
CAS No.:131693-30-6
Molecular Formula:C₁₉H₁₆F₄O₄
Molecular Weight:384.327
Hs Code.:

methyl (<m-(p-methoxytetrafluorobenzyloxy)>-E-3-methyl)cinnamate

Synonyms:

Suppliers and Price of methyl (-E-3-methyl)cinnamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (-E-3-methyl)cinnamate

Chemical Property:

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Technology Process of methyl (-E-3-methyl)cinnamate

There total 4 articles about methyl (-E-3-methyl)cinnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121-71-1
3-Hydroxyacetophenone

: 131693-30-6
methyl (-E-3-methyl)cinnamate

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / aq.NaOH, tetra-n-butylammonium sulfate / CH₂Cl₂ / 3 h / Ambient temperature; similar yield with K₂CO₃ in acetone (reflux, 2 h)

2: 27 percent / xylene / 34 h / Heating

3: 13 percent / Na / 3 h / Ambient temperature

With sodium hydroxide; sodium; tetrabutylammonium sulfate; In dichloromethane; xylene;
DOI:10.1016/S0040-4020(01)87912-6

Reference yield:

: 131693-26-0
m-(pentafluorobenzyloxy)acetophenone

: 131693-30-6
methyl (-E-3-methyl)cinnamate

Guidance literature:: Multi-step reaction with 2 steps

1: 27 percent / xylene / 34 h / Heating

2: 13 percent / Na / 3 h / Ambient temperature

With sodium; In xylene;
DOI:10.1016/S0040-4020(01)87912-6

Reference yield:

: 1765-40-8
(bromomethyl)pentafluorobenzene

: 131693-30-6
methyl (-E-3-methyl)cinnamate

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / aq.NaOH, tetra-n-butylammonium sulfate / CH₂Cl₂ / 3 h / Ambient temperature; similar yield with K₂CO₃ in acetone (reflux, 2 h)

2: 27 percent / xylene / 34 h / Heating

3: 13 percent / Na / 3 h / Ambient temperature

With sodium hydroxide; sodium; tetrabutylammonium sulfate; In dichloromethane; xylene;
DOI:10.1016/S0040-4020(01)87912-6