N-cyclohexyl-3-hydroxy-2-methylenebutyramide

Base Information

Chemical Name:N-cyclohexyl-3-hydroxy-2-methylenebutyramide
CAS No.:78877-65-3
Molecular Formula:C₁₁H₁₉NO₂
Molecular Weight:197.277
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-cyclohexyl-3-hydroxy-2-methylenebutyramide

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Technology Process of N-cyclohexyl-3-hydroxy-2-methylenebutyramide

There total 3 articles about N-cyclohexyl-3-hydroxy-2-methylenebutyramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-91-8,157973-60-9
cyclohexylamine

: 78877-65-3
N-cyclohexyl-3-hydroxy-2-methylenebutyramide

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent / triethylamine / diethyl ether / -78 °C

3: 1.) n-butyl-lithium / 1.) DME, -78 deg C -> room temperature, 60 min, room temperature 30 min, 2.) -78 deg C -> room temperature 15 min

With n-butyllithium; triethylamine; In diethyl ether;

Reference yield:

: 75-07-0,9002-91-9
acetaldehyde

: 78257-87-1
N-cyclohexyl-2-oxopropanamide 2,4,6-tri-iso-propylbenzenesulphonylhydrazone

: 78877-65-3
N-cyclohexyl-3-hydroxy-2-methylenebutyramide

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) DME, -78 deg C -> room temperature, 60 min, room temperature 30 min, 2.) -78 deg C -> room temperature 15 min;

Reference yield:

: 5525-85-9
N-Cyclohexylbrenztraubensaeure-amid

: 78877-65-3
N-cyclohexyl-3-hydroxy-2-methylenebutyramide

Guidance literature:: Multi-step reaction with 2 steps

2: 1.) n-butyl-lithium / 1.) DME, -78 deg C -> room temperature, 60 min, room temperature 30 min, 2.) -78 deg C -> room temperature 15 min

With n-butyllithium;