IrHCl((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2⁽¹⁺⁾*BF₄^(1-)=(IrHCl((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2)BF₄

Base Information

• Chemical Name: IrHCl((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2⁽¹⁺⁾*BF₄^(1-)=(IrHCl((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2)BF₄
• CAS No.: 79292-53-8
• Molecular Formula: BF₄*C₅₂H₄₉ClIrP₄
• Molecular Weight: 1112.33

Synonyms:

Chemical Property of IrHCl((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2⁽¹⁺⁾*BF₄^(1-)=(IrHCl((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2)BF₄

Chemical Property:

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Useful:

Technology Process of IrHCl((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2⁽¹⁺⁾*BF₄^(1-)=(IrHCl((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2)BF₄

There total 4 articles about IrHCl((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2⁽¹⁺⁾*BF₄^(1-)=(IrHCl((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2)BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

IrCl(CO)(((C6H5)2PCH2)2)2(2+)*2BF4(1-) = [IrCl(CO)(((C6H5)2PCH2)2)2](BF4)2 (91606-11-0) → IrHCl((C6H5)2PCH2CH2P(C6H5)2)2(1+)*BF4(1-)=(IrHCl((C6H5)2PCH2CH2P(C6H5)2)2)BF4 (79292-53-8)

Guidance literature:

In [⁽²⁾H₆]acetone; water; (N2), complex dissolved in 2:1 acetone-d6/water at -30°C, warmedto -15°C; not isolated, detected by NMR;

DOI:10.1021/om00122a029

Reference yield:

Ir((C6H5)2PCH2CH2P(C6H5)2)2(1+)*Cl(1-)=Ir((C6H5)2PCH2CH2P(C6H5)2)2Cl (15390-38-2) → IrHCl((C6H5)2PCH2CH2P(C6H5)2)2(1+)*BF4(1-)=(IrHCl((C6H5)2PCH2CH2P(C6H5)2)2)BF4 (79292-53-8)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran

2: dichloromethane

In tetrahydrofuran; dichloromethane;

DOI:10.1021/om00135a025

Reference yield:

tetrafluoroboric acid diethyl ether (67969-82-8) + Ir((C6H5)2PCH2CH2P(C6H5)2)2(1+)*C5H5(1-)*C4H8O=(Ir((C6H5)2PCH2CH2P(C6H5)2)2)C5H5*C4H8O (100228-74-8) → IrHCl((C6H5)2PCH2CH2P(C6H5)2)2(1+)*BF4(1-)=(IrHCl((C6H5)2PCH2CH2P(C6H5)2)2)BF4 (79292-53-8)

Guidance literature:

In dichloromethane; HBF4*OEt2 was added to a soln. of Ir-complex under H2 atmosphere until the colour of the soln. changed from red to light yellow; n-hexane was added, ppt. collected; identified by (1)H NMR and IR spectral data;

DOI:10.1021/om00135a025

upstream raw materials:

tetrafluoroboric acid diethyl ether

Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2⁽¹⁺⁾*C₅H₅^(1-)*C₄H₈O=(Ir((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2)C₅H₅*C₄H₈O

IrCl(CO)(((C₆H₅)2PCH₂)2)2⁽²⁺⁾*2BF₄^(1-) = [IrCl(CO)(((C₆H₅)2PCH₂)2)2](BF₄)2

IrCl(CO)(((C₆H₅)2PCH₂)2)2⁽²⁺⁾*2BF₄^(1-) = [IrCl(CO)(((C₆H₅)2PCH₂)2)2](BF₄)2

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