Octanamide, 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-N-[4-[[2-(phenylmethyl)-2 H-tetrazol-5-yl]methyl]phenyl]-

Base Information

Chemical Name:Octanamide, 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-N-[4-[[2-(phenylmethyl)-2 H-tetrazol-5-yl]methyl]phenyl]-
CAS No.:117897-69-5
Molecular Formula:C23H14F15N5O
Molecular Weight:661.373
Hs Code.:
Mol file:117897-69-5.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Octanamide, 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-N-[4-[[2-(phenylmethyl)-2 H-tetrazol-5-yl]methyl]phenyl]-

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Technology Process of Octanamide, 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-N-[4-[[2-(phenylmethyl)-2 H-tetrazol-5-yl]methyl]phenyl]-

There total 5 articles about Octanamide, 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-N-[4-[[2-(phenylmethyl)-2 H-tetrazol-5-yl]methyl]phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 117293-55-7
Wy 49322

: 117897-69-5
2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-Pentadecafluoro-octanoic acid [4-(2-benzyl-2H-tetrazol-5-ylmethyl)-phenyl]-amide

: 117897-68-4
2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-Pentadecafluoro-octanoic acid [4-(1-benzyl-1H-tetrazol-5-ylmethyl)-phenyl]-amide

Guidance literature:: With potassium carbonate; In acetone; at 50 ℃;
DOI:10.1021/jm00121a003

Reference yield:

: 3544-25-0
p-aminophenylacetonitrile

: 117897-69-5
2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-Pentadecafluoro-octanoic acid [4-(2-benzyl-2H-tetrazol-5-ylmethyl)-phenyl]-amide

Guidance literature:: Multi-step reaction with 3 steps

1: EtOCCH / ethyl acetate / 15 h / 85 °C

2: NaN₃, NH₄Cl / dimethylformamide / 135 °C

3: K₂CO₃ / acetone / 50 °C

With sodium azide; potassium carbonate; ammonium chloride; 1-ethoxyacetylene; In ethyl acetate; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jm00121a003

Reference yield:

: 117897-75-3
2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-Pentadecafluoro-octanoic acid (4-cyanomethyl-phenyl)-amide

: 117897-69-5
2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-Pentadecafluoro-octanoic acid [4-(2-benzyl-2H-tetrazol-5-ylmethyl)-phenyl]-amide

Guidance literature:: Multi-step reaction with 2 steps

1: NaN₃, NH₄Cl / dimethylformamide / 135 °C

2: K₂CO₃ / acetone / 50 °C

With sodium azide; potassium carbonate; ammonium chloride; In N,N-dimethyl-formamide; acetone;
DOI:10.1021/jm00121a003