C₁₄H₁₅NO*ClH

Base Information

• Chemical Name: C₁₄H₁₅NO*ClH
• CAS No.: 1255774-49-2
• Molecular Formula: C₁₄H₁₅NO*ClH
• Molecular Weight: 249.74
• Mol file: 1255774-49-2.mol

Synonyms:

Chemical Property of C₁₄H₁₅NO*ClH

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₄H₁₅NO*ClH

There total 5 articles about C₁₄H₁₅NO*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C14H13NO2 (107947-26-2) → C14H15NO*ClH (1255774-49-2)

Guidance literature:

With ammonium hydroxide; zinc; In water; Sonication;

DOI:10.1002/psc.1279

Reference yield:

4-methoxy-4'-methylbenzophenone (23886-71-7) → C14H15NO*ClH (1255774-49-2)

Guidance literature:

Multi-step reaction with 3 steps

1: boron tribromide / dichloromethane

2: hydroxylamine hydrochloride; potassium hydroxide / ethanol / Reflux

3: ammonium hydroxide; zinc / water / Sonication

With ammonium hydroxide; hydroxylamine hydrochloride; boron tribromide; potassium hydroxide; zinc; In ethanol; dichloromethane; water;

DOI:10.1002/psc.1279

Reference yield:

4-methoxy-benzoyl chloride (100-07-2) → C14H15NO*ClH (1255774-49-2)

Guidance literature:

Multi-step reaction with 4 steps

1: aluminum (III) chloride

2: boron tribromide / dichloromethane

3: hydroxylamine hydrochloride; potassium hydroxide / ethanol / Reflux

4: ammonium hydroxide; zinc / water / Sonication

With aluminum (III) chloride; ammonium hydroxide; hydroxylamine hydrochloride; boron tribromide; potassium hydroxide; zinc; In ethanol; dichloromethane; water;

DOI:10.1002/psc.1279

upstream raw materials:

C₁₄H₁₃NO₂

4-methoxy-4'-methylbenzophenone

4-hydroxy-4'-methylbenzophenone

4-methoxy-benzoyl chloride

Downstream raw materials:

C₂₁H₂₅NO₅

C₁₉H₂₃NO₃