C₁₄H₁₆O₄

Base Information

Chemical Name:C₁₄H₁₆O₄
CAS No.:1449770-02-8
Molecular Formula:C₁₄H₁₆O₄
Molecular Weight:248.279
Hs Code.:

C<sub>14</sub>H<sub>16</sub>O<sub>4</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₆O₄

Chemical Property:

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Technology Process of C₁₄H₁₆O₄

There total 6 articles about C₁₄H₁₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 67-56-1
methanol

: 1449770-14-2
C₁₃H₁₄O₃

: 1449770-02-8
C₁₄H₁₆O₄

Guidance literature:: With sodium hydrogencarbonate; bis-[(trifluoroacetoxy)iodo]benzene; at 0 ℃; for 0.333333h; Inert atmosphere;
DOI:10.1039/c3ob27491h

Reference yield:

: 120743-99-9
p-[(tert-butyldimethylsilyl)oxy]benzaldehyde

: 1449770-02-8
C₁₄H₁₆O₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: titanium tetrachloride; zinc / tetrahydrofuran; dichloromethane; toluene / 0.08 h / 0 °C / Inert atmosphere

1.2: 1 h / Inert atmosphere

2.1: boron trifluoride diethyl etherate; triethylsilane / dichloromethane / 2 h / 0 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

3.2: 20 °C / Inert atmosphere

4.1: triethylamine / dichloromethane / 2 h / 0 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

6.1: bis-[(trifluoroacetoxy)iodo]benzene; sodium hydrogencarbonate / 0.33 h / 0 °C / Inert atmosphere

With triethylsilane; n-butyllithium; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; titanium tetrachloride; sodium hydrogencarbonate; acetic acid; triethylamine; bis-[(trifluoroacetoxy)iodo]benzene; zinc; In tetrahydrofuran; hexane; dichloromethane; toluene;
DOI:10.1039/c3ob27491h

Reference yield:

: 1449770-13-1
C₁₉H₂₈O₃Si

: 1449770-02-8
C₁₄H₁₆O₄

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

2: bis-[(trifluoroacetoxy)iodo]benzene; sodium hydrogencarbonate / 0.33 h / 0 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; sodium hydrogencarbonate; acetic acid; bis-[(trifluoroacetoxy)iodo]benzene; In tetrahydrofuran;
DOI:10.1039/c3ob27491h