dichloro(N-ethoxycarbonylpyrrole-2-thiocarboxamide)bis(triphenylphosphine)iron(II)

Base Information

• Chemical Name: dichloro(N-ethoxycarbonylpyrrole-2-thiocarboxamide)bis(triphenylphosphine)iron(II)
• CAS No.: 122382-02-9
• Molecular Formula: C₄₄H₄₀Cl₂FeN₂O₂P₂S
• Molecular Weight: 849.58
• Mol file: 122382-02-9.mol

Synonyms:

Chemical Property of dichloro(N-ethoxycarbonylpyrrole-2-thiocarboxamide)bis(triphenylphosphine)iron(II)

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of dichloro(N-ethoxycarbonylpyrrole-2-thiocarboxamide)bis(triphenylphosphine)iron(II)

There total 1 articles about dichloro(N-ethoxycarbonylpyrrole-2-thiocarboxamide)bis(triphenylphosphine)iron(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

bis(triphenylphosphine)iron(II) chloride (19543-98-7) + N-ethoxycarbonylpyrrole-2-thiocarboxamide (37488-43-0) → dichloro(N-ethoxycarbonylpyrrole-2-thiocarboxamide)bis(triphenylphosphine)iron(II) (122382-02-9)

Guidance literature:

In benzene; Fe-compd. was dissolved in benzene by warming , addn. of a benzene soln. of ligand ETH, refluxing for 2 h, concentrating of the resulting soln. to half of its volume, addition of petroleum ether yields precipitate; centrifuging of the complexe, washing with petroleum ether (40 - 60°C and 60-80°C), drying in vacuo;

upstream raw materials:

bis(triphenylphosphine)iron(II) chloride

N-ethoxycarbonylpyrrole-2-thiocarboxamide