Technology Process of C9H7BrClF3O
There total 1 articles about C9H7BrClF3O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-butyllithium / hexane; di-isopropyl ether / 0.5 h / -78 °C / Inert atmosphere
1.2: 0.5 h / 20 °C / Inert atmosphere
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C
2.2: 3 h / 20 °C
With
n-butyllithium; tetrabutyl ammonium fluoride;
In
tetrahydrofuran; hexane; di-isopropyl ether;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere
2: dichloromethane; toluene / 8 h / -78 - 25 °C / Inert atmosphere
With
triethylamine;
In
dichloromethane; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triethylamine / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere
2.1: dichloromethane; toluene / 8 h / -78 - 25 °C / Inert atmosphere
3.1: n-butyllithium / hexane; di-isopropyl ether / 0.5 h / -78 °C / Inert atmosphere
3.2: 0.5 h / 20 °C / Inert atmosphere
With
n-butyllithium; triethylamine;
In
hexane; dichloromethane; di-isopropyl ether; toluene;