C₅₉H₈₄FN₉O₁₅

Base Information

Chemical Name:C₅₉H₈₄FN₉O₁₅
CAS No.:1381849-08-6
Molecular Formula:C₅₉H₈₄FN₉O₁₅
Molecular Weight:1178.37
Hs Code.:

C<sub>59</sub>H<sub>84</sub>FN<sub>9</sub>O<sub>15</sub>

Synonyms:

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Chemical Property of C₅₉H₈₄FN₉O₁₅

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Technology Process of C₅₉H₈₄FN₉O₁₅

There total 6 articles about C₅₉H₈₄FN₉O₁₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1381849-03-1
benzyl 2-(4-hydroxy-2-methylbutan-2-yl)-3,5-dimethylphenyl succinate

: 1381849-08-6
C₅₉H₈₄FN₉O₁₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: pyridinium chlorochromate / dichloromethane / 3 h / 20 °C / Inert atmosphere

2.1: sodium dihydrogenphosphate; sodium chlorite; water; dihydrogen peroxide / acetonitrile / 0 - 20 °C / Inert atmosphere

2.2: pH 2 / Inert atmosphere

3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.08 h / 0 °C / Inert atmosphere

3.2: 0 - 20 °C / Inert atmosphere

4.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; water / 3 h / 20 °C

5.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 18 h / 20 °C / Inert atmosphere

6.1: triethylamine / N,N-dimethyl-formamide / 18 h / 20 °C / Inert atmosphere

With sodium chlorite; sodium dihydrogenphosphate; palladium 10% on activated carbon; water; hydrogen; dihydrogen peroxide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmc.2012.04.034

Reference yield:

: 1381849-04-2
benzyl 3,5-dimethyl-2-(2-methyl-4-oxobutan-2-yl)phenyl succinate

: 1381849-08-6
C₅₉H₈₄FN₉O₁₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium dihydrogenphosphate; sodium chlorite; water; dihydrogen peroxide / acetonitrile / 0 - 20 °C / Inert atmosphere

1.2: pH 2 / Inert atmosphere

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.08 h / 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

3.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; water / 3 h / 20 °C

4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 18 h / 20 °C / Inert atmosphere

5.1: triethylamine / N,N-dimethyl-formamide / 18 h / 20 °C / Inert atmosphere

With sodium chlorite; sodium dihydrogenphosphate; palladium 10% on activated carbon; water; hydrogen; dihydrogen peroxide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmc.2012.04.034

Reference yield:

: 1381849-05-3
3-(2-(4-(benzyloxy)-4-oxobutanoyloxy)-4,6-dimethylphenyl)-3-methylbutanoic acid

: 1381849-08-6
C₅₉H₈₄FN₉O₁₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.08 h / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; water / 3 h / 20 °C

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 18 h / 20 °C / Inert atmosphere

4.1: triethylamine / N,N-dimethyl-formamide / 18 h / 20 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2012.04.034